(E)-5-(3,5-Dimethylphenyl)-N-[4-(methylsulfanyl)benzylidene]-1,3,4-thiadiazol-2-amine

被引：2

作者：

Hu, Jun ^{[1
]}

Ji, Jin-xiu ^{[2
]}

Zhou, Ying ^{[3
]}

Wang, Ji-kui ^{[4
]}

Xu, Yan-hua ^{[1
]}

机构：

[1] Nanjing Univ Technol, Dept Safety Engn, Coll Urban Construct & Safety Engn, Nanjing 210009, Peoples R China

[2] Sinochem Jiangsu Corp, Ctr Res & Dev, Nanjing 210002, Peoples R China

[3] Nanjing Univ Technol, Dept Environm Engn, Coll Environm, Nanjing 210009, Peoples R China

[4] Nanjing Univ Technol, Dept Appl Chem, Coll Sci, Nanjing 210009, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

Data-to-parameter ratio = 14.8; Mean σ(C-C) = 0.007 Å; R factor = 0.065; Single-crystal X-ray study; T = 298 K; WR factor = 0.208;

D O I：

10.1107/S1600536810001558

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine and 4-(methylsulfanyl) benzaldehyde. An intramolecular C-H center dot center dot center dot S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 angstrom) five-membered ring. In the crystal structure, intermolecular C-H center dot center dot center dot N hydrogen bonds link the molecules to form layers parallel to (011).

引用

页码：O410 / U2924

页数：10

共 6 条

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[5] A short history of SHELX
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[6] Wang YG, 1999, CHEM J CHINESE U, V20, P1903

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