A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid

被引:138
作者
Umer, Asim [1 ]
Naveed, Shahid [1 ]
Ramzan, Naveed [1 ]
Rafique, Muhammad Shahid [2 ]
Imran, Muhammad [3 ]
机构
[1] Univ Engn & Technol, Dept Chem Engn, Lahore, Pakistan
[2] Univ Engn & Technol, Dept Phys, Lahore, Pakistan
[3] Coll Sci & Technol, Lahore, Pakistan
来源
MATERIA-RIO DE JANEIRO | 2014年 / 19卷 / 03期
关键词
Copper nanoparticles; ascorbic acid; copper salt; XRD; FTIR; REDUCTION; COLLOIDS; CU;
D O I
10.1590/S1517-70762014000300002
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Chemical Reduction technique was employed to prepared highly stable and dispersed Copper nanoparticles using L-Ascorbic Acid (Vitamin C) as reducing as well as capping agent. In this technique, cupric chloride was used as precursor. The effects of different molar ratios of L-Ascorbic Acid on the concentration and size of copper nanoparticles were studied. The Copper nanoparticles were characterized by X-Ray Diffraction, Atomic Absorption Spectrometry, and Fourier Transform Infrared Spectrometry. The results show that with the increase in the molar ratio of L-ascorbic acid the concentration of Copper nanoparticles were also increased. The average particles size of copper nanoparticle was found in the range of 50-60 nm. The product was kept in ambient conditions for three month but no sedimentation or separation was observed. The use of ascorbic acid makes the process a non-toxic, cost effective and environmental friendly green method.
引用
收藏
页码:197 / 203
页数:7
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