Convenient, Solvent-Free Method for Preparation of [Hydroxy(phosphoryloxy)iodo]arenes

被引：2

作者：

Zhu, Min ^{[1
]}

Cai, Cheng Gang ^{[1
]}

Ke, Wei ^{[1
]}

Shao, Jing ^{[1
]}

机构：

[1] Zhejiang Shuren Univ, Coll Biol & Environm Sci, Hangzhou 310015, Zhejiang, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2010年 / 40卷 / 09期

基金：

美国国家科学基金会;

关键词：

Hydroxy(phosphoryloxy)iodo]arenas; preparation; solvent-free; HYPERVALENT IODINE REAGENTS; IODONIUM SALTS; ARYL(2-FURYL)IODONIUM TOSYLATES; ALKYNYLIODONIUM SALTS; ACETYLENIC ESTERS; TERMINAL ALKYNES; <HYDROXY(TOSYLOXY)IODO>BENZENE; CONVERSION; PHOSPHATES; KETONES;

D O I：

10.1080/00397910903097229

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A convenient, solvent-free method for preparation of [hydroxy(phosphoryloxy)iodo]arenes is reported. (Diacetoxyiodo)benzene or other hypervalent iodine reagents and phosphates are simply blended and ground for several minutes in an agate mortar, giving good yields of [hydroxy(phosphoryloxy)iodo]arenes with excellent purities.

引用

页码：1371 / 1376

页数：6

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