Synthesis of 1,4-Dihydropyridines Using Ce(SO4)2-SiO2 as Catalyst under Solvent-free Conditions

被引：10
|
作者：
Pei Wen [1 ]
Wang Qin [1 ]
Li Xiaonian [1 ]
Sun Li [1 ]
机构：
[1] Zhejiang Univ Technol, Coll Chem Engn & Mat, Hangzhou 310014, Zhejiang, Peoples R China
来源：
CHINESE JOURNAL OF CHEMISTRY | 2010年 / 28卷 / 03期
关键词：
1,4-dihydropyridine; Ce(SO4)(2)-SiO2; solvent-free; heterogneous catalysis; supported catalyst; EFFICIENT;
D O I：
10.1002/cjoc.201090101
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A facile and efficient one-pot synthesis of 1,4-dihydropyridines from aldehyde, 1,3-dicarbonyl compounds and ammonium acetate in the presence of Ce(SO4)(2)-SiO2 at 80 degrees C under solvent-free conditions is described. Compared with the classical Hantzsch reaction, this novel method consistently has the advantages of excellent yields and short reaction time.
引用
收藏
页码：483 / 486
页数：4
相关论文
共 50 条
  • [1] PPA-SiO2 Catalyzed One-Pot Synthesis of 1,4-Dihydropyridines Under Solvent-Free Conditions
    Khojastehnezhad, Amir
    Moeinpour, Farid
    Shams, Alireza
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2012, 42 (02) : 273 - 277
  • [2] The solvent-free synthesis of 1,4-dihydropyridines under ultrasound irradiation without catalyst
    Wang, Shu-Xiang
    Li, Zhi-Yan
    Zhang, Jin-Chao
    Li, Ji-Tai
    ULTRASONICS SONOCHEMISTRY, 2008, 15 (05) : 677 - 680
  • [3] Silica supported 12-tungstophosphoric acid catalysts for synthesis of 1,4-dihydropyridines under solvent-free conditions
    Rafiee, Ezzat
    Eavani, Sara
    Rashidzadeh, Solmaz
    Joshaghani, Mohammad
    INORGANICA CHIMICA ACTA, 2009, 362 (10) : 3555 - 3562
  • [4] PEG400-Lithium Carbonate Catalyzed Synthesis of 1,4-Dihydropyridines under Solvent-free Conditions
    Reddy, B. Palakshi
    Rajesh, K.
    Vijayakumar, V.
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2012, 44 (02) : 153 - 158
  • [5] Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones Using Ce(SO4)2-SiO2 as a Heterogeneous and Recyclable Catalyst
    Pei, Wen
    Wang, Qin
    SYNTHETIC COMMUNICATIONS, 2010, 40 (08) : 1209 - 1215
  • [6] An efficient and solvent-free one-pot synthesis of 1,4-dihydropyridines under microwave irradiation
    Kuraitheerthakumaran, A.
    Pazhamalai, S.
    Gopalakrishnan, M.
    CHINESE CHEMICAL LETTERS, 2011, 22 (10) : 1199 - 1202
  • [7] An efficient and solvent-free one-pot synthesis of 1,4-dihydropyridines under microwave irradiation
    A.Kuraitheerthakumaran
    S.Pazhamalai
    M.Gopalakrishnan
    Chinese Chemical Letters, 2011, 22 (10) : 1199 - 1202
  • [8] EFFICIENT AND RAPID HANTZSCH SYNTHESIS OF1,4-DIHYDROPYRIDINES USING A NANO ISOPOLYOXOMOLYBDATE AS A REUSABLE CATALYST UNDER SOLVENT-FREE CONDITION
    Nakhaei, Ahmad
    Yadegarian, Sepideh
    Davoodnia, Abolghasem
    HETEROCYCLIC LETTERS, 2016, 6 (03): : 329 - 339
  • [9] Synthesis of new tripodal Hantzsch 1,4-dihydropyridines under solvent-free condition and their conversion to the corresponding tripodal pyridines
    Zolfigol, Mohammad Ali
    Kolvari, Eskandar
    Abdoli, Abbas
    Shiri, Morteza
    MOLECULAR DIVERSITY, 2010, 14 (04) : 809 - 813
  • [10] Chitosan magnetic nanocomposite: a magnetically reusable nanocatalyst for green synthesis of Hantzsch 1,4-dihydropyridines under solvent-free conditions
    Parichehr Kamalzare
    Behrooz Mirza
    Somayeh Soleimani-Amiri
    Journal of Nanostructure in Chemistry, 2021, 11 : 229 - 243
12345