N-(2-Chlorophenyl)-2,4-dimethylbenzenesulfonamide

被引:2
作者
Gowda, B. Thimme [1 ]
Foro, Sabine [2 ]
Nirmala, P. G. [1 ]
Fuess, Hartmut [2 ]
机构
[1] Mangalore Univ, Dept Chem, Mangalore 574199, India
[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
D O I
10.1107/S1600536810015916
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C(14)H(14)ClNO(2)S, the conformation of the N-C bond in the C-SO(2)-NH-C segment has gauche torsions with respect to the S=O bonds. The molecule is bent at the S atom with a C-SO(2)-NH-C torsion angle of -54.9 (2)degrees. The sulfonyl and aniline benzene rings are rotated relative to each other by 75.7 (1)degrees. An intramolecular N-H center dot center dot center dot Cl hydrogen bond is present. In the crystal, intermolecular N-H center dot center dot center dot O hydrogen-bonding interactions are observed and the molecules are packed into chains parallel to the b axis.
引用
收藏
页码:O1282 / U319
页数:10
相关论文
共 10 条
  • [1] [Anonymous], 2009, CRYSALIS CCD CRYSALI
  • [2] Structural systematics of 4,4′-disubstituted benzenesulfonamidobenzenes.: 1.: Overview and dimerbased isostructures
    Gelbrich, Thomas
    Hursthouse, Michael B.
    Threlfall, Terence L.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2007, 63 (04): : 621 - 632
  • [3] N-(2-Chlorophenyl)-4-methylbenzenesulfonamide
    Gowda, B. Thimme
    Foro, Sabine
    Nirmala, P. G.
    Fuess, Hartmut
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O188 - U2704
  • [4] 2,4-Dimethyl-N-phenylbenzenesulfonamide
    Gowda, B. Thimme
    Foro, Sabine
    Nirmala, P. G.
    Babitha, K. S.
    Fuess, Hartmut
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O576 - U2282
  • [5] 4-Chloro-N-(2-chlorophenyl)-2-methylbenzenesulfonamide
    Gowda, B. Thimme
    Foro, Sabine
    Nirmala, P. G.
    Babitha, K. S.
    Fuess, Hartmut
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O717 - U1672
  • [6] 2,4-Dimethyl-N-(2-methylphenyl)benzenesulfonamide
    Nirmala, P. G.
    Gowda, B. Thimme
    Foro, Sabine
    Fuess, Hartmut
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O3210 - U1626
  • [7] N-(2-chlorophenyl)benzenesulfonamide
    Perlovich, GL
    Tkachev, VV
    Schaper, KJ
    Raevsky, OA
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O780 - O782
  • [8] Savitha M. B., 2006, Z NATURFORSCH A, V60, P600
  • [9] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [10] Structure validation in chemical crystallography
    Spek, Anthony L.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 : 148 - 155