Rapid Characterization of Triterpene Saponins from Zornia brasiliensis by HPLC-ESI-MS/MS

被引：12

作者：

Nascimento, Yuri Mangueira ^{[1
]}

Abreu, Lucas Silva ^{[1
]}

Lima, Ramon Leal ^{[1
]}

Costa, Vicente Carlos O. ^{[1
]}

Miranda de Melo, Jose Iranildo ^{[2
]}

Braz-Filho, Raimundo ^{[3
]}

Silva, Marcelo Sobral ^{[1
]}

Tavares, Josean Fechine ^{[1
]}

机构：

[1] Univ Fed Paraiba, Grad Program Nat & Synthet Bioact Prod, Hlth Sci Ctr, BR-58051900 Joao Pessoa, Paraiba, Brazil

[2] Ctr Biol & Hlth Sci, Grad Program Ecol & Conservat, Dept Biol, BR-58429500 Campina Grande, Paraiba, Brazil

[3] Darcy Ribeiro Norte Fluminense State Univ, Ctr Sci & Technol, BR-28013600 Rio De Janeiro, Brazil

来源：

MOLECULES | 2019年 / 24卷 / 14期

关键词：

triterpene saponins; soyasaponins; Zornia brasiliensis; HPLC-DAD-ESI-MS; MS; PERFORMANCE LIQUID-CHROMATOGRAPHY; WISTARIA-BRACHYBOTRYS SIEB; LEGUMINOUS PLANTS; SOYASAPOGENOL-A; ESSENTIAL OIL; SOYASAPONINS; QUANTIFICATION; CONSTITUENTS; GLYCOSIDES; ISOFLAVONES;

D O I：

10.3390/molecules24142519

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Zornia brasiliensis Vogel (Leguminosae) is a species popularly known in Brazil as urinaria, urinana, and carrapicho, it is popularly used as a diuretic and in the treatment of venereal diseases. A specific methodology to obtain a saponin-enriched fraction and high-performance liquid chromatography coupled with diode array detection, ion trap mass spectrometry, and TOF-MS (HPLC-DAD-ESI-MS/MS) was applied for the analysis of triterpene saponins. The MS and MS/MS experiments were carried out by ionization in negative mode. Molecular mass and fragmentation data were used to support the structural characterization of the saponins. Based on retention times, high-resolution mass determination and fragmentation, 35 oleanane-triterpene saponins were tentatively identified in Z. brasiliensis.

引用

页数：14

共 50 条

[41] Selenium speciation analysis of Misgurnus anguillicaudatus selenoprotein by HPLC-ICP-MS and HPLC-ESI-MS/MS
Gong, Like
Xu, Qingbing
Lee, Charles
Zhang, Hong
EUROPEAN FOOD RESEARCH AND TECHNOLOGY, 2012, 235 (01) : 169 - 176
[42] Dynamics of Zebrafish Heart Regeneration Using an HPLC-ESI-MS/MS Approach
Ma, Danjun
Tu, Chengan
Sheng, Quanhu
Yang, Yuxi
Kan, Zhisheng
Guo, Yan
Shyr, Yu
Scott, Ian C.
Lou, Xin
JOURNAL OF PROTEOME RESEARCH, 2018, 17 (03) : 1300 - 1308
[43] HPLC-ESI-MS/MS检测蜂蜜中林可霉素残留
阮祥春
曾明华
赵明
安徽农业科学, 2009, 37 (05) : 1889 - 1891
[44] Characterization of alkyl thiosulfinate in Allium hookeri root using HPLC-ESI-MS
Dong Young Rhyu
Si Hyung Park
Journal of the Korean Society for Applied Biological Chemistry, 2013, 56 : 457 - 459
[45] Characterization of the effects of β-carotene on the thermal oxidation of triacylglycerols using HPLC-ESI-MS
Zeb, Alam
Murkovic, Michael
EUROPEAN JOURNAL OF LIPID SCIENCE AND TECHNOLOGY, 2010, 112 (11) : 1218 - 1228
[46] Application of HPLC-ICP-MS and HPLC-ESI-MS procedures for arsenic speciation in seaweeds
Jiang, S.-J. (sjjiang@faculty.nsysu.edu.tw), 1600, American Chemical Society (60):
[47] Characterization and quantification of the triterpenoids in different parts of Xanthoceras sorbifolia by HPLC-ESI-MS
Ling, Junhong
Liu, Lili
Wang, Yixiang
Li, Zeyun
Liu, Ran
Li, Qing
Wang, Yi
Yang, Baizhen
Chen, Xiaohui
Bi, Kaishun
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2011, 55 (02) : 259 - 264
[48] HPLC-DAD and HPLC-ESI-MS/MS methods for metabolite profiling of propolis extracts
Pellati, Federica
Orlandini, Giulia
Pinetti, Diego
Benvenuti, Stefania
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2011, 55 (05) : 934 - 948
[49] Characterization of Alkyl Thiosulfinate in Allium hookeri Root Using HPLC-ESI-MS
Rhyu, Doug Young
Park, Si Hyung
JOURNAL OF THE KOREAN SOCIETY FOR APPLIED BIOLOGICAL CHEMISTRY, 2013, 56 (04): : 457 - 459
[50] Application of HPLC-ICP-MS and HPLC-ESI-MS Procedures for Arsenic Speciation in Seaweeds
Hsieh, Yu-Jhe
Jiang, Shiuh-Jen
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2012, 60 (09) : 2083 - 2089

← 1 2 3 4 5 →