Development and Validation of High-Performance Thin-Layer Chromatographic-Fingerprint Analysis of Stemona sessilifolia (Miq.) Miq. with the Reference of Protostemonine

被引：1
|
作者：
Tao, Ye [2 ]
Zhang, Yazhong [1 ]
机构：
[1] Anhui Inst Food & Drug Control, Hefei 230051, Peoples R China
[2] Anhui Univ Chinese Med, Hefei 230031, Peoples R China
来源：
JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC | 2015年 / 28卷 / 06期
关键词：
High-performance thin-layer chromatography; Fingerprint; Protostemonine; Stemona sessilifolia (Miq.) Miq; MASS-SPECTROMETRY; RADIX STEMONAE; ALKALOIDS; ROOTS;
D O I：
10.1556/1006.2015.28.6.5
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A high-performance thin-layer chromatographic (HPTLC) method for the analysis of the protostemonine from Stemona sessilifolia (Miq.) Miq. has been developed and validated. According to the HPTLC fingerprint, 12 common peaks were selected to evaluate the similarities among 10 batches of samples with R-F values ranging from 0.02 to 0.95. Ten different batches of samples were stable and reliable in quality, all the similarities of which are more than 0.98. The results indicated that this method was sensitive and precise for the quality evaluation of S. sessilifolia samples.
引用
收藏
页码：448 / 451
页数：4
相关论文
共 50 条
12345