Development and Validation of High-Performance Thin-Layer Chromatographic-Fingerprint Analysis of Stemona sessilifolia (Miq.) Miq. with the Reference of Protostemonine

被引：1
|
作者：
Tao, Ye [2 ]
Zhang, Yazhong [1 ]
机构：
[1] Anhui Inst Food & Drug Control, Hefei 230051, Peoples R China
[2] Anhui Univ Chinese Med, Hefei 230031, Peoples R China
来源：
JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC | 2015年 / 28卷 / 06期
关键词：
High-performance thin-layer chromatography; Fingerprint; Protostemonine; Stemona sessilifolia (Miq.) Miq; MASS-SPECTROMETRY; RADIX STEMONAE; ALKALOIDS; ROOTS;
D O I：
10.1556/1006.2015.28.6.5
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A high-performance thin-layer chromatographic (HPTLC) method for the analysis of the protostemonine from Stemona sessilifolia (Miq.) Miq. has been developed and validated. According to the HPTLC fingerprint, 12 common peaks were selected to evaluate the similarities among 10 batches of samples with R-F values ranging from 0.02 to 0.95. Ten different batches of samples were stable and reliable in quality, all the similarities of which are more than 0.98. The results indicated that this method was sensitive and precise for the quality evaluation of S. sessilifolia samples.
引用
收藏
页码：448 / 451
页数：4
相关论文
共 50 条
  • [1] Development and Validation of High-Performance Thin-Layer Chromatographic—Fingerprint Analysis of Stemona sessilifolia (Miq.) Miq. with the Reference of Protostemonine
    Ye Tao
    Yazhong Zhang
    JPC – Journal of Planar Chromatography – Modern TLC, 2015, 28 : 448 - 451
  • [2] Development and Validation of a High-Performance Thin-Layer Chromatographic Fingerprint Method for the Evaluation of QiYi Capsules with the Reference of Myotonin
    Wang, Fang
    Meng, Mei
    Chen, Li
    Wang, Xiaoyu
    Sun, Qing
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2014, 27 (03) : 199 - 203
  • [3] Development and Validation of a High-Performance Thin-Layer Chromatographic Fingerprint Method for the Evaluation of QiYi Capsules with the Reference of Myotonin
    Fang Wang
    Mei Meng
    Li Chen
    Xiaoyu Wang
    Qing Sun
    JPC – Journal of Planar Chromatography – Modern TLC, 2014, 27 : 199 - 203
  • [4] Development and validation of a high-performance thin-layer chromatographic—densitometric method for the analysis of miconazole in creams
    Nelson E. Masota
    Prosper Tibalinda
    Raphael Shedafa
    Joseph Sempombe
    Eliangiringa A. Kaale
    JPC – Journal of Planar Chromatography – Modern TLC, 2016, 29 : 469 - 473
  • [5] Development and Validation of a High-Performance Thin-Layer Chromatographic-Densitometric Method for the Analysis of Miconazole in Creams
    Masota, Nelson E.
    Tibalinda, Prosper
    Shedafa, Raphael
    Sempombe, Joseph
    Kaale, Eliangiringa A.
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2016, 29 (06) : 469 - 473
  • [6] Fingerprint Analysis and the Application of High-Performance Thin-Layer Chromatography for the Quality Assessment of QiYi Capsules with the Reference of Tripterygium wilfordii
    Zhang, He
    Meng, Mei
    Chen, Li
    Wang, Fang
    Zhang, Jing
    Jiang, Ying
    Wang, Wen
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2015, 28 (03) : 218 - 222
  • [7] Fingerprint Analysis and the Application of High-Performance Thin-Layer Chromatography for the Quality Assessment of QiYi Capsules with the Reference of Tripterygium wilfordii
    He Zhang
    Mei Meng
    Li Chen
    Fang Wang
    Jing Zhang
    Ying Jiang
    Wen Wang
    JPC – Journal of Planar Chromatography – Modern TLC, 2015, 28 : 218 - 223
  • [8] Development of Two High-Performance Thin-Layer Chromatographic Methods for the Determination of Irbesartan in Tablets and Plasma
    Hussein, Samiha Abd El-Rahman
    Abd El-Wadood, Hanaa Mohamed
    Abdallah, Mohamed Abou-Elwafa
    Khorshed, Ahmed Abd El-Hamid
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2015, 28 (01) : 83 - 89
  • [9] Development and Validation of a High-Performance Thin-Layer Chromatographic—Densitometric Method for the Quantification of Swertiamarin in Traditional Bitters and Formulations
    Javed Ahamad
    Naila Hassan
    Saima Amin
    Showkat R. Mir
    JPC – Journal of Planar Chromatography – Modern TLC, 2015, 28 : 61 - 66
  • [10] High-Performance Thin-Layer Chromatographic Analysis of Bicalutamide in Bulk Drug and Liposomes
    Subramanian, Ganesa Sundararajan
    Karthik, Arumugam
    Baliga, Ashok
    Musmade, Prashant
    Kini, Suvarna
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2009, 22 (04) : 273 - 276
12345