Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) of ZnS1-xSex semiconductor materials

被引：6
|
作者：
Gruhl, S
Vogt, C
Vogt, J
Hotje, U
Binnewies, M
机构：
[1] Leibniz Univ Hannover, Inst Inorgan Chem, D-30167 Hannover, Germany
[2] Univ Leipzig, Inst Expt Phys 2, D-04103 Leipzig, Germany
来源：
MICROCHIMICA ACTA | 2005年 / 149卷 / 1-2期
关键词：
quantification; laser ablation ICP-MS; zinc sulphide selenide; gradient; chemical vapour transport reaction;
D O I：
10.1007/s00604-004-0287-2
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Luminous zinc sulphide selenide crystals (ZnS1-xSex) with an anion-gradient in the mum-range within the crystal were quantitatively investigated by LA-ICP-MS. Reference standard crystals were synthesized by chemical vapour transport reaction and characterized by mu-XRF, SEM, PIXE, RBS and solution ICP-MS. Values from several analytical methods were then combined to describe the concentration in the reference crystals. Using these crystals, calibration curves with high correlation coefficients could be obtained for laser ablation ICP-MS determination of elemental concentrations. The gradient determined afterwards in the zinc sulphide selenide sample crystals was in the order of 30 wt% in Se-content within an 800 mum distance. This shows the promising capabilities of LA-ICP-MS in the field of elemental quantification in the mum-range.
引用
收藏
页码：43 / 48
页数：6
相关论文
共 50 条
  • [1] Biomonitoring of hair samples by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Sela, H.
    Karpas, Z.
    Zoriy, M.
    Pickhardt, C.
    Becker, J. S.
    INTERNATIONAL JOURNAL OF MASS SPECTROMETRY, 2007, 261 (2-3) : 199 - 207
  • [2] Synthesis of PGE sulfide standards for laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Cora C. Wohlgemuth-Ueberwasser
    Chris Ballhaus
    Jasper Berndt
    Vaida Stotter née Paliulionyte
    Thomas Meisel
    Contributions to Mineralogy and Petrology, 2007, 154 : 607 - 617
  • [3] Synthesis of PGE sulfide standards for laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Wohlgemuth-Ueberwasser, Cora C.
    Ballhaus, Chris
    Berndt, Jasper
    Paliulionyte, Vaida Stotter Nee
    Meisel, Thomas
    CONTRIBUTIONS TO MINERALOGY AND PETROLOGY, 2007, 154 (05) : 607 - 617
  • [4] Imaging of nutrient elements in the leaves of Elsholtzia splendens by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Wu, Bei
    Zoriy, Miroslav
    Chen, Yingxu
    Becker, J. Sabine
    TALANTA, 2009, 78 (01) : 132 - 137
  • [5] IMAGING ELEMENT-DISTRIBUTION PATTERNS IN MINERALS BY LASER ABLATION - INDUCTIVELY COUPLED PLASMA - MASS SPECTROMETRY (LA-ICP-MS)
    Ulrich, Thomas
    Kamber, Balz S.
    Jugo, Pedro J.
    Tinkham, Doug K.
    CANADIAN MINERALOGIST, 2009, 47 (05) : 1001 - 1012
  • [6] Laser-Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS): setting operating conditions and instrumental performance
    D'Oriano, Claudia
    Da Pelo, Stefania
    Podda, Francesca
    Cioni, Raffaello
    PERIODICO DI MINERALOGIA, 2008, 77 (03): : 65 - 75
  • [7] Elemental mapping in fossil tooth root section of Ursus arctos by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Vasinova Galiova, M.
    Fisakova, M. Nyvltova
    Kynicky, J.
    Prokes, L.
    Neff, H.
    Mason, A. Z.
    Gadas, P.
    Kosler, J.
    Kanicky, V.
    TALANTA, 2013, 105 : 235 - 243
  • [8] Biomonitoring of metal contamination in a marine prosobranch snail (Nassarius reticulatus) by imaging laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
    Santos, Mirian C.
    Wagner, Martin
    Wu, Bei
    Scheider, Jessica
    Oehlmann, Joerg
    Cadore, Solange
    Becker, J. Sabine
    TALANTA, 2009, 80 (02) : 428 - 433
  • [9] Reproducibility of laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) measurements in mussel shells and Comparison with micro-drill sampling and solution ICP-MS
    Anh Tuan Phung
    Baeyens, Willy
    Leermakers, Martine
    Goderis, Steven
    Vanhaecke, Frank
    Gao, Yue
    TALANTA, 2013, 115 : 6 - 14
  • [10] Inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation ICP-MS for isotope analysis of long-lived radionuclides
    Becker, JS
    INTERNATIONAL JOURNAL OF MASS SPECTROMETRY, 2005, 242 (2-3) : 183 - 195
12345