Preparation and properties of the AEO9/alcohol/alkane/water reverse microemulsion ceramic inks

被引:16
作者
Guo, RS [1 ]
Qi, HT [1 ]
Yang, ZF [1 ]
Chen, Y [1 ]
机构
[1] Tianjin Univ, Minist Educ, Key Lab Adv Ceram & Machining Technol, Tianjin 300072, Peoples R China
基金
中国国家自然科学基金;
关键词
powders : chemical preparation; suspensions; electrical conductivity; ZrO2; ceramic ink;
D O I
10.1016/j.ceramint.2003.12.009
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Reverse microemulsion method was applied and the AEO(9)/alcohol/alkane/water system was chosen to prepare ceramic inks for forming by jet-printing. The ceramic inks were prepared by reaction after mixing the zirconium oxychloride and ammonia reverse microemulsions homogeneously through vigorous stirring. The physicochemical properties of the ZrO2 ceramic inks were systematically determined and discussed based on the requirements of the ink-jet printers available. They generally met the requirements for the drop on demand printers and were adjusted and improved by adding a small amount of alcohol and inorganic electrolyte to meet the demands for continuous ink-jet printers. It was shown that the ceramic ink with viscosity below 18 mPa s and conductivity close to 100 mS m(-1) was obtained after modification. Transmission electron microscope observation showed that ZrO2 nanoparticles in the reverse microemulsion were very well dispersed and the stability of the inks was excellent. Besides, several ceramic ink compositions with bicontinuous structure were specially designed based on the phase diagram, and the changes of water-dissolving amount into the system was investigated aiming to increase the concentration of ZrO2 ceramic ink. (C) 2004 Elsevier Ltd and Techna S.r.l. All rights reserved.
引用
收藏
页码:2259 / 2267
页数:9
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