Comparison of soluble manganese(IV) and acidic potassium permanganate chemiluminescence detection using flow injection and sequential injection analysis for the determination of ascorbic acid in Vitamin C tablets

被引：58

作者：

Anastos, N ^{[1
]}

Barnett, NW ^{[1
]}

Hindson, BJ ^{[1
]}

Lenehan, CE ^{[1
]}

Lewis, SW ^{[1
]}

机构：

[1] Deakin Univ, Ctr Chiral & Mol Technol, Sch Biol & Chem Sci, Geelong, Vic 3217, Australia

来源：

TALANTA | 2004年 / 64卷 / 01期

关键词：

flow injection analysis; sequential injection analysis; Vitamin C;

D O I：

10.1016/j.talanta.2004.01.021

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The limits of detection (3s) for ascorbic acid were 5 x 10(-8) M with acidic potassium permanganate using both flow injection analysis (FIA) and sequential injection analysis (SIA) whereas the soluble manganese(IV) afforded 1 x 10(-8) M and 5 x 10(-9) M for FIA and SIA, respectively. Determinations of ascorbic acid in Vitamin C tablets were achieved with minimal sample pretreatment using a standard additions calibration and gave good agreement with those of iodimetric titration. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：130 / 134

页数：5

共 49 条

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