Synthesis of Glycyrrhetinic Acid Monoglycoside by Hydrolysis of Glycyrrhizic Acid in Subcritical Water

被引：3

作者：

Filonova, O. V. ^{[1
]}

Lekar, A. V. ^{[1
]}

Borisenko, S. N. ^{[1
]}

Maksimenko, E. V. ^{[1
]}

Vetrova, E. V. ^{[1
]}

Borisenko, N. I. ^{[1
]}

Minkin, V. I. ^{[1
]}

机构：

[1] Southern Fed Univ, Inst Phys & Organ Chem, Rostov Na Donu, Russia

来源：

RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B | 2015年 / 9卷 / 08期

关键词：

ammonium glycyrrhizinate; Glycyram; glycyrrhizic acid; glycyrrhetinic acid; glycyrrhetinic acid monoglycoside; electrospray ionization mass spectrometry; HPLC-MS; subcritical water;

D O I：

10.1134/S1990793115080035

中图分类号：

O64 [物理化学（理论化学）、化学物理学]; O56 [分子物理学、原子物理学];

学科分类号：

070203 ; 070304 ; 081704 ; 1406 ;

摘要：

A method for the synthesis of glycyrrhetinic acid monoglycoside by hydrolysis of glycyrrhizic acid in subcritical water at temperatures ranging between 100 and 300 degrees C is under development. The maximum yield of the target product is achieved at 160 degrees C.

引用

页码：1153 / 1156

页数：4

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