A mild approach to the synthesis of sn-glycerol 1,2-di-γ-linolenate 3-palmitate

被引：0

作者：

Rejzek, M

Vacek, M

Wimmer, Z

机构：

[1] Acad Sci Czech Republ, Inst Organ Chem & Biochem, CZ-16610 Prague 6, Czech Republic

[2] Inst Chem Technol, CZ-16028 Prague 6, Czech Republic

来源：

HELVETICA CHIMICA ACTA | 2000年 / 83卷 / 10期

关键词：

D O I：

10.1002/1522-2675(20001004)83:10<2756::AID-HLCA2756>3.0.CO;2-I

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A synthetic approach comprising several studied modifications was applied to the preparation of sn-glycerol 1,2-di-gamma -linolenate 3-palmitate (4). Thereby, a convenient and mild synthetic method was elaborated. affording 4 from 1,2-O-isopropylidene-sn-glycerol (1) in an average yield of 65-75% and analytically acceptable purity.

引用

页码：2756 / 2760

页数：5

共 14 条

[11] Comparison of the Grignard deacylation TLC and HPLC methods and high resolution C-13-NMR for the sn-2 positional analysis of triacylglycerols containing gamma-linolenic acid [J].