X-ray absorption spectroscopy beamline at the Siam Photon Laboratory

被引:0
作者
Klysubun, Wantana [1 ]
Tarawarakam, Pongjakr [1 ]
Sombunchoo, Panidtha [1 ]
Klinkhieo, Supat [1 ]
Chaiprapa, Jitrin [1 ]
Songsiriritthigul, Prayoon [1 ,2 ]
机构
[1] Natl Synchrotron Res Ctr, 111 Univ Ave,Muang Dist, Nakhon Rachasima 30000, Thailand
[2] Suranaree Univ Tech, Sch Phys, Nakhon Rachasima 30000, Thailand
来源
SYNCHROTRON RADIATION INSTRUMENTATION, PTS 1 AND 2 | 2007年 / 879卷
关键词
X-ray beamline; X-ray absorption spectroscopy; low-energy x-rays;
D O I
暂无
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A bending magnet beamline has been constructed and commissioned for x-ray absorption spectroscopy (XAS) at the Siam Photon Laboratory. The photon energy is tunable from 1830 eV to 8000 eV using a Lemmonier-type, fixed-exit double crystal monochromator equipped with InSb(111), Si(111), Ge(220) crystals. Elemental K-edges are then accessible from silicon to iron. A series of low conductance vacuum tubes has been designed and installed between the pumping chambers in the front end to obtain the proper pressure difference between the upstream and the downstream of the front end. Thus lower-energy photons, around K-edges of silicon, phosphorous, and sulfur, can be delivered to the experimental XAS station without being absorbed by a window. In this report, the design of the beamline is described. The commissioning results including the measured photon flux at sample and experimental XAS spectra are presented.
引用
收藏
页码:860 / +
页数:2
相关论文
共 8 条
[1]   Sulfur K-shell photoabsorption spectroscopy of the sulfanes R-Sn-R, n=2-4 [J].
Chauvistre, R ;
Hormes, J ;
Hartmann, E ;
Etzenbach, N ;
Hosch, R ;
Hahn, J .
CHEMICAL PHYSICS, 1997, 223 (2-3) :293-302
[2]  
Farrell SP, 2002, AM MINERAL, V87, P1321
[3]   XAFS study of adsorbed and mineral forms of phosphate [J].
Hesterberg, D ;
Zhou, WQ ;
Hutchison, KJ ;
Beauchemin, S ;
Sayers, DE .
JOURNAL OF SYNCHROTRON RADIATION, 1999, 6 :636-638
[4]   HIGH-VACUUM 2 CRYSTAL SOFT-X-RAY MONOCHROMATOR [J].
LEMONNIER, M ;
COLLET, O ;
DEPAUTEX, C ;
ESTEVA, JM ;
RAOUX, D .
NUCLEAR INSTRUMENTS & METHODS, 1978, 152 (01) :109-111
[5]   Quantitative speciation of sulfur in bacterial sulfur globules:: X-ray absorption spectroscopy reveals at least three different species of sulfur [J].
Prange, A ;
Chauvistré, R ;
Modrow, H ;
Hormes, J ;
Trüper, HG ;
Dahl, C .
MICROBIOLOGY-SGM, 2002, 148 :267-276
[6]   X-ray absorption spectroscopy and its application in biological, agricultural and environmental research [J].
Prange A. ;
Modrow H. .
Reviews in Environmental Science and Biotechnology, 2002, 1 (4) :259-276
[7]   Characterization of sulfur in asphaltenes by sulfur K- and L-edge XANES spectroscopy [J].
Sarret, G ;
Connan, J ;
Kasrai, M ;
Eybert-Bérard, L ;
Bancroft, GM .
JOURNAL OF SYNCHROTRON RADIATION, 1999, 6 :670-672
[8]   Sulfur K-edge XANES spectroscopy as a tool for understanding sulfur dynamics in soil organic matter [J].
Solomon, D ;
Lehmann, J ;
Martínez, CE .
SOIL SCIENCE SOCIETY OF AMERICA JOURNAL, 2003, 67 (06) :1721-1731