Complete assignments of the 1H and 13C resonances of 40-epi-(N1-tetrazolyl)rapamycin and revised 13C assignments for rapamycin

被引：11

作者：

Pagano, TG ^{[1
]}

机构：

[1] Abbott Labs, Global Pharmaceut R&D Div, Abbott Pk, IL 60064 USA

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 2005年 / 43卷 / 02期

关键词：

NMR; H-1; C-13; two-dimensional NMR; rapamycin; 40-epi-(N1-tetrazolyl)-rapamycin; ABT-578;

D O I：

10.1002/mrc.1524

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Complete H-1 and C-13 assignments of 40-epi-(N1-tetrazolyl)-rapamycin (ABT-578) in DMSO-d(6) were made using H-1, C-13, DQCOSY, ROESY, TOCSY, HSQC and HMBC spectra. Comparing the assignments with those of rapamycin showed that in the published C-13 assignments of rapamycin in DMSO-d(6) the shifts for C-12 and C-42 have been interchanged, as well as the shifts for C-1 and C-8. Copyright (C) 2004 John Wiley Sons, Ltd.

引用

页码：174 / 175

页数：2

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