Collecting 3D electron diffraction data by the rotation method

被引：271

作者：

Zhang, Daliang ^{[1
,2
]}

Oleynikov, Peter ^{[1
]}

Hovmoller, Sven ^{[1
]}

Zou, Xiaodong ^{[1
]}

机构：

[1] Stockholm Univ, Dept Mat & Environm Chem, S-10691 Stockholm, Sweden

[2] Jilin Univ, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS | 2010年 / 225卷 / 2-3期

关键词：

Electron diffraction; Data collection; 3D diffraction data; PRECESSION TECHNIQUE; MICROSCOPY; BEAM; CRYSTALLOGRAPHY; INTENSITIES; SYSTEM; PHASE; MODEL; AREA;

D O I：

10.1524/zkri.2010.1202

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

A new method for collecting complete three-dimensional electron diffraction data is described. Diffraction data is collected by combining electron beam tilt at many very small steps, with rotation of the crystal in a few but large steps. A number of practical considerations are discussed, as well as advantages and disadvantages compared to other methods of collecting electron diffraction data.

引用

页码：94 / 102

页数：9

共 22 条

[1]

Arndt U.W., 1977, The Rotation Method in Crystallography: Data Collection from Macromolecular Crystals

[2] Precession technique and electron diffractometry as new tools for crystal structure analysis and chemical bonding determination [J].

Avilov, A. ;

Kuligin, K. ;

Nicolopoulos, S. ;

Nickolskiy, M. ;

Boulahya, K. ;

Portillo, J. ;

Lepeshov, G. ;

Sobolev, B. ;

Collette, J. P. ;

Martin, N. ;

Robins, A. C. ;

Fischione, P. .

ULTRAMICROSCOPY, 2007, 107 (6-7) :431-444

[3] Structure of the polycrystalline zeolite catalyst IM-5 solved by enhanced charge flipping [J].

Baerlocher, Christian ;

Gramm, Fabian ;

Massueger, Lars ;

McCusker, Lynne B. ;

He, Zhanbing ;

Hovmoeller, Sven ;

Zou, Xiaodong .

SCIENCE, 2007, 315 (5815) :1113-1116

[4] NEW GTB-TYPE THALLIUM NIOBATE [J].

BHIDE, V ;

GASPERIN, M .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1979, 35 (JUN) :1318-1321

[5] A practical method to detect and correct for lens distortion in the TEM [J].

Capitani, GC ;

Oleynikov, P ;

Hovmöller, S ;

Mellini, M .

ULTRAMICROSCOPY, 2006, 106 (02) :66-74

[6]

Cowley J.M., 1992, Electron Diffraction Techniques, V1

[7]

Dorset Douglas, 1995, STRUCTURAL ELECTRON CRYSTALLOGRAPHY

[8]

GEMMI M, 2001, ELECT CRYSTALLOGGRAP

[9] Structure model for the phase AlmFe derived from three-dimensional electron diffraction intensity data collected by a precession technique.: Comparison with convergent-beam diffraction [J].

Gjonnes, J ;

Hansen, V ;

Berg, BS ;

Runde, P ;

Cheng, YF ;

Gjonnes, K ;

Dorset, DL ;

Gilmore, CJ .

ACTA CRYSTALLOGRAPHICA SECTION A, 1998, 54 :306-319

[10] Complex zeolite structure solved by combining powder diffraction and electron microscopy [J].

Gramm, Fabian ;

Baerlocher, Christian ;

McCusker, Lynne B. ;

Warrender, Stewart J. ;

Wright, Paul A. ;

Han, Bada ;

Hong, Suk Bong ;

Liu, Zheng ;

Ohsuna, Tetsu ;

Terasaki, Osamu .

NATURE, 2006, 444 (7115) :79-81

← 1 2 3 →