Self-assembly of α-Fe2O3 nanoparticles into rice ball shaped microstructures via a pyrolytic route

被引:5
作者
Cheng, Zhipeng [1 ]
Xu, Jiming [1 ]
Zhong, Hui [1 ]
Yang, Yi [2 ]
Chen, Weifan [3 ]
机构
[1] Huaiyin Normal Univ, Jiangsu Key Lab Chem Low Dimens Mat, Huaian 223300, Peoples R China
[2] Nanjing Univ Sci & Technol, Natl Special Superfine Powder Engn Res Ctr, Nanjing 210094, Peoples R China
[3] Nanchang Univ, Sch Mat Sci & Engn, Nanchang 330031, Peoples R China
基金
中国国家自然科学基金;
关键词
Nanomaterials; Microstructure; alpha-Fe2O3; Self-assembly; THERMAL-DECOMPOSITION; NANORODS; NANOCRYSTALS;
D O I
10.1016/j.spmi.2009.11.005
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Rice ball shaped alpha-Fe2O3 microstructures have been synthesized using a single-step Fe(NO3)(3) solution calcination route without the assistance of any other additions. A series of techniques, including XRD, XPS, FE-SEM and DLS ones, were used to characterize the product. Thermogravimetric (TG) analysis provided insight into the decomposition process of the Fe(NO3)(3) precursor. A possible growth mechanism of the rice ball shaped alpha-Fe2O3 microstructures was explained. (C) 2009 Elsevier Ltd. All rights reserved.
引用
收藏
页码:253 / 258
页数:6
相关论文
共 16 条
[1]   Facile synthesis of single crystalline α-Fe2O3 ellipsoidal nanoparticles and its catalytic performance for removal of carbon monoxide [J].
Hu, Chaoquan ;
Gao, Zhenghong ;
Yang, Xiaorui .
MATERIALS CHEMISTRY AND PHYSICS, 2007, 104 (2-3) :429-433
[2]   Synthesis and characterization of novel nanostructured fishbone-like Cu(OH)2 and CuO from Cu4SO4(OH)6 [J].
Jia, Wenzhao ;
Reitz, Eliot ;
Sun, Hui ;
Zhang, Heng ;
Lei, Yu .
MATERIALS LETTERS, 2009, 63 (05) :519-522
[3]   Thermal decomposition synthesis of 3D urchin-like α-Fe2O3 superstructures [J].
Jiao Hua ;
Yang Heqing .
MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS, 2009, 156 (1-3) :68-72
[4]   Preparation and characterization of α-Fe2O3 polyhedral nanocrystals via annealing technique [J].
Kumar, Rajesh ;
Gautam, S. ;
Hwang, In-Chul ;
Lee, Jae Rhung ;
Chae, K. H. ;
Thakur, Nagesh .
MATERIALS LETTERS, 2009, 63 (12) :1047-1050
[5]  
KURTZ RL, 1983, SURF SCI LETT, V129, P243
[6]   Versatile synthesis of rectangular shaped nanobat-like CuO nanostructures by hydrothermal method; structural properties and growth mechanism [J].
Li, Fei ;
Tao, Kong ;
Wentuan, Bi ;
Li, Dachang ;
Li, Zhen ;
Huang, Xintang .
APPLIED SURFACE SCIENCE, 2009, 255 (12) :6279-6284
[7]   Electrochemical performance of α-Fe2O3 nanorods as anode material for lithium-ion cells [J].
Liu, Hao ;
Wang, Guoxiu ;
Park, Jinsoo ;
Wang, Jiazhao ;
Liu, Huakun ;
Zhang, Chao .
ELECTROCHIMICA ACTA, 2009, 54 (06) :1733-1736
[8]   Surfactant-assisted synthesis of α-Fe2O3 nanotubes and nanorods with shape-dependent magnetic properties [J].
Liu, Lu ;
Kou, Hui-Zhong ;
Mo, Wenling ;
Liu, Huajie ;
Wang, Yuqiu .
JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (31) :15218-15223
[9]   Preparation and,characterization of shuttle-like α-Fe2O3 nanoparticles by supermolecular template [J].
Liu, XM ;
Fu, SY ;
Xiao, HM ;
Huang, CJ .
JOURNAL OF SOLID STATE CHEMISTRY, 2005, 178 (09) :2798-2803
[10]   Facile route to the synthesis of porous α-Fe2O3 nanorods [J].
Mandal, Saikat ;
Mueller, Axel H. E. .
MATERIALS CHEMISTRY AND PHYSICS, 2008, 111 (2-3) :438-443