Determination of Dry Matter Content in Potato Tubers by Low-Field Nuclear Magnetic Resonance (LF-NMR)

被引:82
作者
Hansen, Christian Lyndgaard [1 ]
Thybo, Anette Kistrup [2 ]
Bertram, Hanne Christine [2 ]
Viereck, Nanna [1 ]
van den Erg, Frans [1 ]
Engelsen, Soren Balling [1 ]
机构
[1] Univ Copenhagen, Dept Food Sci, Fac Life Sci, DK-1958 Frederiksberg C, Denmark
[2] Aarhus Univ, Dept Food Sci, Fac Agr Sci, DK-5792 Aarslev, Denmark
关键词
Low-field NMR; potato; PLS regression; dry matter content; DoubleSlicing; specific gravity; core consistency; NEAR-INFRARED SPECTROSCOPY; SOLANUM-TUBEROSUM; CURVE RESOLUTION; SENSORY TEXTURE; RELAXATION DATA; H-1-NMR; QUALITY; WATER; PREDICTION; COOKING;
D O I
10.1021/jf101319q
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
The objective of this study was to develop a calibration model between time-domain low-field nuclear magnetic resonance (LF-NMR) measurements and dry matter (DM) content in single potatoes. An extensive sampling procedure was used to collect 210 potatoes from eight cultivars with a wide range in DM content, ranging from 16 to 28%. The exponential NMR relaxation curves were resolved into four mono-exponential components using a number of solution diagnostics. Partial least-squares (PLS) regression between NMR parameters (relaxation time constants T(2,1-4) and magnitudes M(0,1-4)) and DM content resulted in a model with low error (RMSECV, 0.71; RMSEP, 0.60) and high correlation (r(cv), 0.97; r(test), 0.98) between predicted and actual DM content. Correlation between DM content and each of the proton populations revealed that M0,1 (T(2,1), 3.6 ms; SD, 0.3 ms; r, 0.95) and M(0.4) (T(2,4), 508 ms; SD, 53 ms; r, -0.90) were the major contributors to the PLS regression model.
引用
收藏
页码:10300 / 10304
页数:5
相关论文
共 31 条
[1]   DOUBLESLICING: A non-iterative single profile multi-exponential curve resolution procedure - Application to time-domain NMR transverse relaxation data [J].
Andrade, Leticia ;
Micklander, Elisabeth ;
Farhat, Imad ;
Bro, Rasmus ;
Engelsen, Soren Balling .
JOURNAL OF MAGNETIC RESONANCE, 2007, 189 (02) :286-292
[2]  
[Anonymous], P C MATR PENC
[3]   Comparative chemometric analysis of transverse low-field 1H NMR relaxation data [J].
Bechmann, IE ;
Pedersen, HT ;
Norgaard, L ;
Engelsen, SB .
ADVANCES IN MAGNETIC RESONANCE IN FOOD SCIENCE, 1999, (231) :217-225
[4]  
Behrend P, 1880, LANDWIRTSCHAFTLICHEN, V25, P107
[5]  
Belton P. S., 1990, Comments on Agricultural and Food Chemistry, V2, P179
[6]  
Berendsen H. J. C., 1992, Trends in Food Science & Technology, V3, P202, DOI 10.1016/0924-2244(92)90190-8
[7]  
BURTON WG, 1989, POTATO, P392
[8]  
BURTON WG, 1989, POTATO, P142
[9]   EFFECTS OF DIFFUSION ON FREE PRECESSION IN NUCLEAR MAGNETIC RESONANCE EXPERIMENTS [J].
CARR, HY ;
PURCELL, EM .
PHYSICAL REVIEW, 1954, 94 (03) :630-638
[10]   PowerSlicing [J].
Engelsen, SB ;
Bro, R .
JOURNAL OF MAGNETIC RESONANCE, 2003, 163 (01) :192-197