Synthesis, characterization and X-ray crystal structure of Zn-II complex with poly-nitrogen ligand [eta(3)-HB(3,5-Me(2)pz)(3)]Zn-2 center dot 2C(6)H(5)CH(3)

被引：0
作者：
Yang, KW
Wang, YZ
Huang, ZX
Sun, J
机构：
[1] FUDAN UNIV,DEPT CHEM,SHANGHAI 200433,PEOPLES R CHINA
[2] ACAD SINICA,SHANGHAI INST ORGAN CHEM,SHANGHAI 200032,PEOPLES R CHINA
来源：
POLYHEDRON | 1997年 / 16卷 / 08期
关键词：
synthesis; characterization; crystal structure; zinc complex; poly-nitrogen ligand;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Di-hydrotris(3,5-dimethylpyrazo-1-yl)borate Zn-II was prepared from KHB(3,5-Me(2)pz)(3) and Zn(NO3)(2) . 6H(2)O(-) in acetone, characterized by elemental analysis and H-1 NMK. Crystal structure determination shows that the configuration around the Zn-II center is a slightly distorted octahedron. Copyright (C) 1997 Elsevier Science Ltd.
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页码：1297 / 1300
页数：4
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