Development of a buoyancy material of hollow glass microspheres/SiO2 for high-temperature application

被引:21
作者
Ren, Sue [1 ]
Hu, Xiaoxia [1 ]
Ren, Haitao [1 ]
Wang, Mingchao [1 ]
Guo, Anran [1 ]
Liu, Jiachen [1 ]
Du, Haiyan [1 ]
Xian, Liang [1 ]
机构
[1] Tianjin Univ, Sch Mat Sci & Engn, Key Lab Adv Ceram & Mech Technol, Minist Educ, Tianjin 300072, Peoples R China
关键词
SiO2; Temperature resistance; Hollow glass microspheres; Buoyancy material; Compressive strength; MECHANICAL-PROPERTIES; PRECERAMIC POLYMER; FRACTURE STRENGTH; SYNTACTIC FOAMS; YOUNGS MODULUS; SILICONE RESIN; CERAMIC FOAMS; FILMS;
D O I
10.1016/j.jallcom.2017.06.002
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A type of buoyancy material with excellent temperature resistance was successfully prepared through a molding method, and the hollow glass microspheres (HGMs) and silicon oxide (SiO2) were used as the filler and the matrix, respectively. The effect of sintering temperature on mechanical performance, microstructure, and high-temperature performance of the HGMs/SiO2 composite were investigated in the study. The HGMs/SiO2 composite exhibited low density (0.47-0.53 g/cm(3)), high porosity (66.7-75.6%), low thermal conductivity (0.18-0.27 W/(m circle K)), and relatively high compressive strength (3.8-5.2 MPa) properties. The values of Weibull moduli m used to predict the variation degree of compressive strength during the compression process was in the range of 5-15 and its values for the samples sintered at 850 degrees C was 14.64. Two stages namely elastic stage and fracture stage were shown in the stress-strain curves and in the elastic stage, the stress increased linearly with increasing of the strain until reaching the maximum stress. In the fracture stage, the sample gradually destroyed with further increasing of the strain until complete failure. The compressive strength of the HGMs/SiO2 composites tested at high-temperature was larger than that of the one tested at room temperature. The HGMs/SiO2 composite exhibited low density, low thermal conductivity and excellent temperature resistance properties and can be used as the structural material or buoyancy material in the deep sea field in the near future. (C) 2017 Elsevier B.V. All rights reserved.
引用
收藏
页码:213 / 219
页数:7
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