Boric Acid Supported on Montmorillonites as Catalysts for Synthesis of 2,3-dihydroquinazolin-4(1H)-ones

被引：0
|
作者：
Kancherla, Mahesh [1 ]
Katlakanti, Mohan Reddy [2 ]
Seku, Kondaiah [3 ]
Badathala, Vijayakumar [1 ]
机构：
[1] Vel Tech High Tech Dr Rangarajan Dr Sakunthala En, Dept Chem, Chennai 600062, Tamil Nadu, India
[2] UPES, Coll Engn Studies, Dept Chem, Bidholi Campus, Dehra Dun 248007, India
[3] Shinas Coll Technol, Dept Chem, Shinas, Oman
来源：
IRANIAN JOURNAL OF CHEMISTRY & CHEMICAL ENGINEERING-INTERNATIONAL ENGLISH EDITION | 2019年 / 38卷 / 04期
关键词：
Clays; catalysts; H3BO3/mont K10; H3BO3/mont K30; 2,3-dihydroquinazolin-4(1H)-ones; ONE-POT SYNTHESIS; EFFICIENT SYNTHESIS; SUBSTITUTED 2,3-DIHYDROQUINAZOLINE-4(1H)-ONES; HETEROGENEOUS CATALYST; REUSABLE CATALYST; WATER; DERIVATIVES; GREEN; 1,2-DIHYDROQUINAZOLIN-4(3H)-ONES; NANOCATALYST;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Synthesis of 2,3-dihydroquinazolin-4(1H)-ones using H3BO3/montmorillonite K10 (H3BO3/mont K10) catalyst has been reported. H3BO3/mont K10 and H3BO3/mont K30 have been prepared and used as catalysts in the reaction between anthranilamide and benzaldehyde to prepare 2-phenyl-2,3-dihydroquinazolin-4(1H)-one. The catalysts have been characterized for their physico-chemical properties by XRD, IR, BET surface analysis, TGA, SEM, and DRIFTS. H3BO3/mont K10 has shown better catalytic activity among the catalysts tested for the synthesis of 2-phenyl-2,3-dihydroquinazolin-4(1H)-one. The reaction conditions have been optimized for 2-phenyl-2,3-dihydroquinazolin-4(1H)-one and the reusability of H3BO3/mont K10 has also been investigated. Several 2,3-dihydroquinazolin-4(1H)-one derivatives have been synthesized in good to excellent yields using the optimized reaction conditions.
引用
收藏
页码：37 / 49
页数：13
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