Simultaneous determination of beauvericin, enniatins, and fusaproliferin by high performance liquid chromatography

被引：39
作者：
Monti, SM
Fogliano, V
Logrieco, A
Ferracane, R
Ritieni, A [1 ]
机构：
[1] Univ Naples Federico II, Dipartimento Sci Alimento, I-80055 Parco Gussone Portici, Italy
[2] CNR, Ist Tossine & Micotossine Parassiti Vegetali, I-70125 Bari, Italy
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2000年 / 48卷 / 08期
关键词：
beauvericin; enniatin; fusaproliferin; HPLC; Fusarium;
D O I：
10.1021/jf990373n
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
A rapid, sensitive and inexpensive HPLC method for routine screening ofbeauvericin, fusaproliferin, and enniatin B-1, A(1), and B has been optimized. Detection limits were determined, ranging between 0.5 and 3.6 ng according to the compound obtained after spiking samples with each mycotoxin at 10-56 mu g/mL concentration range; recoveries averaging from 56 to 74% were obtained. LC-MS conditions for enniatin analyses by API electrospray technique were set up, this allowing a unique identification of three different enniatins.
引用
收藏
页码：3317 / 3320
页数：4
相关论文
共 27 条
[1]  
[Anonymous], 9102 RIKILTDLO
[2]   TUMORIGENICITY OF CITRININ IN MALE F344 RATS [J].
ARAI, M ;
HIBINO, T .
CANCER LETTERS, 1983, 17 (03) :281-287
[3]  
Busby Jr WF, 1984, CHEM CARCINOGENS, P945
[4]   THE INSECTICIDAL ACTIVITY OF BEAUVERICIN AND THE ENNIATIN COMPLEX [J].
GROVE, JF ;
POPLE, M .
MYCOPATHOLOGIA, 1980, 70 (02) :103-105
[5]   ISOLATION OF BEAUVERICIN AS AN INSECT TOXIN FROM FUSARIUM-SEMITECTUM AND FUSARIUM-MONILIFORME VAR SUBGLUTINANS [J].
GUPTA, S ;
KRASNOFF, SB ;
UNDERWOOD, NL ;
RENWICK, JAA ;
ROBERTS, DW .
MYCOPATHOLOGIA, 1991, 115 (03) :185-189
[6]   ANTIBIOTIC POLYPEPTIDES - BIOSYNTHESIS ON MULTIFUNCTIONAL PROTEIN TEMPLATES [J].
KLEINKAUF, H .
PLANTA MEDICA, 1979, 35 (01) :1-18
[7]  
Kostecki M., 1995, Microbiologie, Aliments, Nutrition, V13, P67
[8]  
KRSKA R, 1997, J AGR FOOD CHEM, V44
[9]   Fusaproliferin production by Fusarium subglutinans and its toxicity to Artemia salina, SF-9 insect cells, and IARC/LCL 171 human B lymphocytes [J].
Logrieco, A ;
Moretti, A ;
Fornelli, F ;
Fogliano, V ;
Ritieni, A ;
Caiaffa, MF ;
Randazzo, G ;
Bottalico, A ;
Macchia, L .
APPLIED AND ENVIRONMENTAL MICROBIOLOGY, 1996, 62 (09) :3378-3384
[10]   NATURAL OCCURRENCE OF BEAUVERICIN IN PREHARVEST FUSARIUM-SUBGLUTINANS INFECTED CORN EARS IN POLAND [J].
LOGRIECO, A ;
MORETTI, A ;
RITIENI, A ;
CHELKOWSKI, J ;
ALTOMARE, C ;
BOTTALICO, A ;
RANDAZZO, G .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1993, 41 (11) :2149-2152
123