Simultaneous determination of beauvericin, enniatins, and fusaproliferin by high performance liquid chromatography

被引：39
作者：
Monti, SM
Fogliano, V
Logrieco, A
Ferracane, R
Ritieni, A [1 ]
机构：
[1] Univ Naples Federico II, Dipartimento Sci Alimento, I-80055 Parco Gussone Portici, Italy
[2] CNR, Ist Tossine & Micotossine Parassiti Vegetali, I-70125 Bari, Italy
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2000年 / 48卷 / 08期
关键词：
beauvericin; enniatin; fusaproliferin; HPLC; Fusarium;
D O I：
10.1021/jf990373n
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
A rapid, sensitive and inexpensive HPLC method for routine screening ofbeauvericin, fusaproliferin, and enniatin B-1, A(1), and B has been optimized. Detection limits were determined, ranging between 0.5 and 3.6 ng according to the compound obtained after spiking samples with each mycotoxin at 10-56 mu g/mL concentration range; recoveries averaging from 56 to 74% were obtained. LC-MS conditions for enniatin analyses by API electrospray technique were set up, this allowing a unique identification of three different enniatins.
引用
收藏
页码：3317 / 3320
页数：4
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