An efficient and convenient procedure for the synthesis of 2-alkyl-2-alkoxy-1,2-di(furan-2-yl)ethanone under ultrasound in the presence of solid-liquid phase transfer catalysis conditions

被引:4
作者
Zhang, Feng
Sun, Jikui
Gao, Dawei
Li, Yazhuo
Zhang, Yumin
Zhao, Tianqi
Chen, Xiaodong
机构
[1] Jilin Univ, Coll Chem, Changchun 130012, Peoples R China
[2] Jilin Univ, Expt Ctr Testing Sci, Changchun 130023, Peoples R China
关键词
ultrasound; phase transfer catalysis; alkyl halides; furoin; alkylation;
D O I
10.1016/j.ultsonch.2007.02.004
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
Irradiation with ultrasound is found to facilitate the synthesis of 2-alkyl-2- alkoxy-1, 2-di(furan-2-yl)ethanone in the presence of tetrabutylammonium bromide (TBAB) as solid-liquid phase transfer catalysis. A higher yields (> 70%) and shorter reaction time (< 15 min) give this method obvious advantages over the conventional ones. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:493 / 496
页数:4
相关论文
共 10 条
[1]  
Autorenkollektiv, 1977, ORGANIKUM
[2]  
DEHMLOW SS, 1993, PHASE TRANSFER CATAL
[3]  
EINHORN C, 1989, SYNTHESIS-STUTTGART, P787
[4]  
FENG Z, IN PRESS CHEM RES CH
[5]  
GAO DW, 1998, FINE CHEM CHINA, V15, P49
[6]   Ultrasound promoted C-alkylation of benzyl cyanide - effect of reactor and ultrasound parameters [J].
Hofmann, J ;
Freier, U ;
Wecks, M .
ULTRASONICS SONOCHEMISTRY, 2003, 10 (4-5) :271-275
[7]  
MASON TJ, 1991, CHEM CHEM ENG
[8]   Phase transfer catalysis: Chemistry and engineering [J].
Naik, SD ;
Doraiswamy, LK .
AICHE JOURNAL, 1998, 44 (03) :612-646
[9]  
QIAO QD, 1997, FINE CHEM CHINA, V14, P32
[10]   Ultrasound promoted N-alkylation of pyrrole using potassium superoxide as base in crown ether [J].
Yim, ES ;
Park, MK ;
Han, BH .
ULTRASONICS SONOCHEMISTRY, 1997, 4 (02) :95-98