Sulfamic-acid-catalyzed simple and efficient synthesis of 4-aryl-3-methyl-1-phenyl-1H-benzo[g] pyrazolo[3,4-b] quinoline-5,10-diones under solvent-free conditions

被引：17

作者：

Wu, Liqiang ^{[1
]}

Ma, Suying ^{[1
]}

Yan, Fulin ^{[1
]}

Yang, Chunguang ^{[1
]}

机构：

[1] Xinxiang Med Univ, Sch Pharm, Xinxiang 453003, Henan, Peoples R China

来源：

MONATSHEFTE FUR CHEMIE | 2010年 / 141卷 / 05期

关键词：

Pyrazolo[3,4-b]quinoline; Sulfamic acid; One-pot synthesis; Solvent-free; ONE-POT SYNTHESIS; MICROWAVE IRRADIATION; DERIVATIVES;

D O I：

10.1007/s00706-010-0282-8

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An efficient synthesis of 4-aryl-3-methyl-1-phenyl-1H-benzo[g]pyrazolo[3,4-b] quinoline-5,10-diones from the three-component condensation reaction of 3-methyl-1-phenyl-1H-pyrazol-5-amine, aromatic aldehydes, and 2-hydroxy-1,4-naphthoquinone under solvent-free conditions in good to excellent yields and short reaction times using sulfamic acid as heterogeneous acid catalyst has been investigated.

引用

页码：565 / 568

页数：4

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