X-Ray diffraction and high resolution NMR analysis of methyl D-glucopyranuronate derivatives

被引：9
|
作者：
Trynda, A
Madaj, J
Konitz, A
Wisniewski, A
机构：
[1] Univ Gdansk, Dept Chem, PL-80952 Gdansk, Poland
[2] Gdansk Tech Univ, Dept Inorgan Chem, PL-80952 Gdansk, Poland
来源：
CARBOHYDRATE RESEARCH | 2000年 / 329卷 / 01期
关键词：
D-glucuronic acid derivatives; x-ray diffraction; H-1; NMR; C-13;
D O I：
10.1016/S0008-6215(00)00157-9
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
X-Ray diffraction and high resolution H-1 and C-13 NMR spectral data for methyl 2,3,4,-tri-O-acetyl-alpha-D-glucopyranuronate and methyl (allyl 2,3,4-tri-O-acetyl-beta-D-glucopyranosid)uronate are presented. Both compounds adopt the C-4(1) conformation. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：249 / 252
页数：4
相关论文
共 50 条
  • [1] X-ray diffraction and high resolution NMR spectroscopy analysis of methyl β-D-glucofuranosidurono-6,3-lactone
    Madaj, J
    Trynda, A
    Konitz, A
    Nowacki, A
    Wisniewski, A
    CARBOHYDRATE RESEARCH, 1998, 308 (3-4) : 431 - 433
  • [2] X-ray diffraction and high-resolution NMR spectroscopy of methyl 3-azido-2,3-dideoxy-α-D-lyxo-hexopyranoside
    Liberek, B
    Sikorski, A
    Melcer, A
    Konitz, A
    CARBOHYDRATE RESEARCH, 2003, 338 (08) : 795 - 799
  • [3] High-resolution X-ray diffraction datasets: Carbonates
    Amao, Abduljamiu O.
    Al-Otaibi, Bandar
    Al-Ramadan, Khalid
    DATA IN BRIEF, 2022, 42
  • [4] High-resolution X-ray diffraction from microstructures
    Chrosch, J
    Salje, EKH
    FERROELECTRICS, 1997, 194 (1-4) : 149 - 159
  • [5] NMR assignments and single-crystal X-ray diffraction analysis of deoxyloganic acid
    Teng, RW
    Wang, DZ
    Wu, YS
    Lu, Y
    Zheng, QT
    Yang, CR
    MAGNETIC RESONANCE IN CHEMISTRY, 2005, 43 (01) : 92 - 96
  • [6] High resolution X-ray diffraction studies on hexaphenyl thin films
    Resel, R
    Leising, G
    SURFACE SCIENCE, 1998, 409 (02) : 302 - 306
  • [7] Analyzing shear band formation with high resolution X-ray diffraction
    Pagan, Darren C.
    Obstalecki, Mark
    Park, Jun-Sang
    Miller, Matthew P.
    ACTA MATERIALIA, 2018, 147 : 133 - 148
  • [8] High resolution X-ray diffraction using energy resolving detectors
    Meyer, DC
    Seidel, A
    Richter, K
    Paufler, P
    EPDIC 7: EUROPEAN POWDER DIFFRACTION, PTS 1 AND 2, 2001, 378-3 : 200 - 205
  • [9] High-resolution X-ray diffraction imaging in a tabletop system
    Greenberg, Joel A.
    Dudley, Colt
    Moody, Ryan
    Richmond, Turner
    Espenhahn, Eric
    Pike, Daniel
    Kida, Sakurako
    Kapadia, Anuj J.
    Coccarelli, David
    ANOMALY DETECTION AND IMAGING WITH X-RAYS, ADIX IX, 2024, 13043
  • [10] Chemical bond secrets as revealed by high resolution X-ray diffraction
    Lecomte, Claude
    Bendeif, El-Eulmi
    Pillet, Sebastien
    ACTUALITE CHIMIQUE, 2011, (356-57): : 118 - 122
12345