Orthorhombic Polymorphism of 4-(2-Phenyldiazenyl)-2-[(phenylimino)methyl]phenol

被引:0
|
作者
Suda, Shintaro [1 ]
Onami, Yuika [1 ]
Haraguchi, Tomoyuki [1 ]
Akitsu, Takashiro [1 ]
机构
[1] Tokyo Univ Sci, Fac Sci, Dept Chem, Shinjuku Ku, 1-3 Kagurazaka, Tokyo 1628601, Japan
来源
X-RAY STRUCTURE ANALYSIS ONLINE | 2021年 / 37卷
关键词
D O I
暂无
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the title compound, 4-(2-phenyldiazenyl)-2-[(phenylimino)methyl]phenol, was determined to be an orthorhombic system, Pna2(1), with cell parameters a = 18.351(4)angstrom, b = 17.574(4)angstrom, c = 4.5721(9)angstrom, V = 1474.5(5)angstrom(3), Z = 4, at 173 K. It was a polymorphism of the previously reported monoclinic system measured at 293 K. This orthorhombic molecule took a more planar shape than the monoclinic one, and did not exhibit intramolecular hydrogen bonds in the crystal.
引用
收藏
页码:17 / 18
页数:2
相关论文
共 50 条
  • [31] 4-{[2-(2,4-Dinitrophenyl)hydrazinylidene]methyl}phenol ethanol hemisolvate
    Zhai, Xiu-Rong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O3142 - U341
  • [32] 2-[4-(Dimethylamino)benzylideneimino]phenol
    Wang, Qiang
    Wang, Da-Qi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4838 - U6254
  • [33] Photoswitching Properties of 5-Methoxy-2-(2-phenyldiazenyl) Pyridine
    Foy, Justin T.
    Ta, Nicholas
    Hoyt, Johnathon
    Staples, Richard J.
    Ehm, Christian
    CHEMISTRYSELECT, 2022, 7 (47):
  • [34] 2-{[2-(4-Chlorophenyl)hydrazinylidene]methyl}phenol
    Lo, Kong Mun
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1452 - U1014
  • [35] CRYSTAL DATA FOR 2-(4-METHYL-2-PYRIDYLIMINOMETHYL)PHENOL AND 2-(4,6-DIMETHYL-2-PYRIDYLIMINO-METHYL)PHENOL
    ESCOBAR, C
    GARLAND, MT
    SPODINE, E
    JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1983, 16 (APR) : 276 - 276
  • [36] 2-({[4-(1,3-Benzothiazol-2-yl)phenyl]amino}methyl)phenol
    Potgieter, Kim
    Gerber, Thomas
    Hosten, Eric
    Betz, Richard
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O27 - +
  • [37] 2-[(4-Methoxyanilino)methyl]phenol
    Shu, Hong
    Yu, Ning-Shu
    Xie, Guo-Lan
    Chen, Li-Zhuang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2304 - U2365
  • [38] 2-[(4-Chloroanilino)methyl]phenol
    Chen, Li-Zhuang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2125 - U1327
  • [39] Synthesis, characterization and antimicrobial studies of 2-{(E)-[(2-hydroxy-5-methylphenyl)imino]methyl}-4-[(E)-phenyldiazenyl] phenol as a novel azo-azomethine dye
    Kose, Muhammet
    Kurtoglu, Nurcan
    Gumussu, Ozkan
    Tutak, Mustafa
    McKee, Vickie
    Karakas, Duran
    Kurtoglu, Mukerrem
    JOURNAL OF MOLECULAR STRUCTURE, 2013, 1053 : 89 - 99
  • [40] 2-{(E)-[(3-Iodo-4-methylphenyl) imino]methyl}-4-(trifluoromethoxy) phenol
    Pekdemir, Merve
    Isik, Samil
    Agar, Aysen Alaman
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2148 - +