Synthesis and characterization of silica nanoparticles

被引:7
作者
Aghababazadeh, R. [1 ]
Tabatabaei, S. [1 ,2 ]
Shokuhfar, A. [2 ]
Mirhabibi, A. R. [1 ,3 ]
机构
[1] Iran Color Res Ctr, Ceram Engn Dept, Banihashem Sq E End Hemmat High Way,32 Afshari, Tehran, Iran
[2] KNT Univ Technol, Dept Mech Engn, Tehran, Iran
[3] Iran Univ Sci & Technol, Dept Mat, Tehran, Iran
来源
NANOSCIENCE AND TECHNOLOGY, PTS 1 AND 2 | 2007年 / 121-123卷
关键词
silica; nanoparticles; colloidal stability; structology;
D O I
10.4028/www.scientific.net/SSP.121-123.49
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Currently there are several models discussed to describe the formation of monodispersed silica particles. Monodisperse colloidal silica was prepared from tetraethoxysilane in mixture of ammonia, water and ethanol. Chemical system reaction permits the controlled growth of silica nanoparticles and subsequent condition of silicic acid in alcoholic solution. The molar ratio of NH4OH, C2H5OH and H2O has a significant effect on particle size and specific surface area of silica particles. The nature of particles was evaluated using X-ray diffraction, energy dispersive spectroscopy (EDS) and BET. The morphology of particles were determined by scanning electron microscopy (SEM) and transmission electron microscopy(TEM).
引用
收藏
页码:49 / 52
页数:4
相关论文
共 13 条
[1]   Particulate sol-gel route for microporous silica gels [J].
Chu, L ;
TejedorTejedor, MI ;
Anderson, MA .
MICROPOROUS MATERIALS, 1997, 8 (5-6) :207-213
[2]   Size, volume fraction, and nucleation of Stober silica nanoparticles [J].
Green, DL ;
Lin, JS ;
Lam, YF ;
Hu, MZC ;
Schaefer, DW ;
Harris, MT .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2003, 266 (02) :346-358
[3]   Chemical reaction kinetics leading to the first Stober silica nanoparticles - NMR and SAXS investigation [J].
Green, DL ;
Jayasundara, S ;
Lam, YF ;
Harris, MT .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 2003, 315 (1-2) :166-179
[4]  
GREGG SJ, 1990, ADSORPTION SURFACE A
[5]   THE SOL-GEL PROCESS [J].
HENCH, LL ;
WEST, JK .
CHEMICAL REVIEWS, 1990, 90 (01) :33-72
[6]   Synthesis and characterization of nanosilica prepared by precipitation method [J].
Jal, PK ;
Sudarshan, M ;
Saha, A ;
Patel, S ;
Mishra, BK .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2004, 240 (1-3) :173-178
[7]   Experimental study of synthesis of silica nanoparticles by a bench-scale diffusion flame reactor [J].
Jang, HD .
POWDER TECHNOLOGY, 2001, 119 (2-3) :102-108
[8]  
KOZAKURA T, 1974, Patent No. 49036876
[9]   Preparation and characterization of nano-structured silica from rice husk [J].
Liou, TH .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2004, 364 (1-2) :313-323
[10]   Synthesis of oxide nanoparticles in low pressure flames [J].
Skandan, G ;
Chen, YJ ;
Glumac, N ;
Kear, BH .
NANOSTRUCTURED MATERIALS, 1999, 11 (02) :149-158