Sonochemical synthesis of two new nano lead(II) coordination polymers: Evaluation of structural transformation via mechanochemical approach

被引：11

作者：

Aboutorabi, Leila ^{[1
]}

Morsali, Ali ^{[1
]}

机构：

[1] Tarbiat Modares Univ, Fac Basic Sci, Dept Chem, POB 14115-175, Tehran, Iran

来源：

ULTRASONICS SONOCHEMISTRY | 2016年 / 32卷

关键词：

Coordination polymers; Sonochemical method; Structural transformations; Mechanochemistry; REMOVAL;

D O I：

10.1016/j.ultsonch.2016.01.023

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

Two new lead(II) mixed-ligand coordination polymers, [Pb(PNO)(SCN)](n), (1) and [Pb(PNO)(N-3)](n) (2), (HPNO = picolinic acid N-oxide) were synthesized by a sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy and elemental analysis. Compounds 1 and 2 were structurally characterized by single crystal X-ray diffraction. The thermal behavior of 1 and 2 were studied by thermal gravimetric analysis. Structural transformations of compounds 1 and 2 were evaluated through anion-replacement processes by mechanochemical method. Moreover, the effect of sonication conditions including time, concentrations of initial reagents and power of irradiation were evaluated on size and morphology of compounds 1 and 2. (C) 2016 Elsevier B.V. All rights reserved.

引用

页码：31 / 36

页数：6

共 9 条

[1] Liquid phase adsorption by microporous coordination polymers: Removal of organosulfur compounds
Cychosz, Katie A.
Wong-Foy, Antek G.
Matzger, Adam J.
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2008, 130 (22) : 6938 - +
[2] Nanomedicine Applications of Hybrid Nanomaterials Built from Metal-Ligand Coordination Bonds: Nanoscale Metal-Organic Frameworks and Nanoscale Coordination Polymers
He, Chunbai
Liu, Demin
Lin, Wenbin
[J]. CHEMICAL REVIEWS, 2015, 115 (19) : 11079 - 11108
[3] Assembly of Cd(II) coordination polymers: structural variation, supramolecular isomers, and temperature/anion-induced solvent-mediated structural transformations
Hou, Shuang-Shuang
Huang, Xuan
Guo, Jun-Gu
Zheng, Sheng-Run
Lei, Jing
Tan, Jing-Bo
Fan, Jun
Zhang, Wei-Guang
[J]. CRYSTENGCOMM, 2015, 17 (04): : 947 - 959
[4] Lead(II) carboxylate supramolecular compounds: Coordination modes, structures and nano-structures aspects
Hu, Mao-Lin
Morsali, Ali
Aboutorabi, Leila
[J]. COORDINATION CHEMISTRY REVIEWS, 2011, 255 (23-24) : 2821 - 2859
[5] Luminescent Microporous Metal-Organic Framework with Functional Lewis Basic Sites on the Pore Surface: Specific Sensing and Removal of Metal Ions
Jayaramulu, Kolleboyina
Narayanan, Raghu Pradeep
George, Subi J.
Maji, Tapas Kumar
[J]. INORGANIC CHEMISTRY, 2012, 51 (19) : 10089 - 10091
[6] Chemistry of coordination space of porous coordination polymers
Kitagawa, Susumu
Matsuda, Ryotaro
[J]. COORDINATION CHEMISTRY REVIEWS, 2007, 251 (21-24) : 2490 - 2509
[7] Dynamic structural transformations of coordination supramolecular systems upon exogenous stimulation
Li, Cheng-Peng
Chen, Jing
Liu, Chun-Sen
Du, Miao
[J]. CHEMICAL COMMUNICATIONS, 2015, 51 (14) : 2768 - 2781
[8] Single-Crystal to Single-Crystal Photochemical Structural Transformations of Interpenetrated 3D Coordination Polymers by [2+2] Cycloaddition Reactions
Mir, Mohammad Hedayetullah
Koh, Lip Lin
Tan, Geok Kheng
Vittal, Jagadese J.
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2010, 49 (02) : 390 - 393
[9] Porous Phosphorescent Coordination Polymers for Oxygen Sensing
Xie, Zhigang
Ma, Liqing
deKrafft, Kathryn E.
Jin, Athena
Lin, Wenbin
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2010, 132 (03) : 922 - +

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