Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

被引：0
作者：
Zhang, JG [1 ]
Zhang, TL
Yu, KB
机构：
[1] Beijing Inst Technol, Dept Mech Engn, Beijing 100081, Peoples R China
[2] Chinese Acad Sci, Chengdu Branch, Ctr Anal & Measurement, Chengdu 610041, Peoples R China
来源：
KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII | 2003年 / 04期
关键词：
4-amino-1,2,4-triazol-5-one; molecular structure; crystal structure; structure characterization;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
4-Amino-1,2,4-triazol-5-one hydrate (ATO.H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to triclinic crystal system, space group P (1) over bar with crystal parameters of a = 6.432(1) Angstrom, b = 6.551(1) Angstrom, c = 6340(1) Angstrom, alpha = 68.04(1)degrees, beta = 82.18(1)degrees, gamma = 81.90(1)degrees, V = 259.7(7) Angstrom(3), Z = 2, D-c = 1.5 10 g/cm(3), mu = 0. 131 mm(-1), F(000) = 124. ATO.H2O was characterized by FT-IR analysis, X-ray diffraction analysis and single crystal diffraction analysis.
引用
收藏
页码：542 / 547
页数：6
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