Mapping strain fields induced in Zr-based bulk metallic glasses during in-situ nanoindentation by X-ray nanodiffraction

被引:12
作者
Gamcova, J. [1 ,6 ]
Mohanty, G. [2 ]
Michalik, S. [3 ,7 ]
Wehrs, J. [2 ]
Bednarcik, J. [1 ]
Krywka, C. [4 ]
Breguet, J. M. [2 ,5 ]
Michler, J. [2 ]
Franz, H. [1 ]
机构
[1] DESY, Notkestr 85, D-22547 Hamburg, Germany
[2] Empa, Lab Mech Mat & Nanostruct, Swiss Fed Labs Mat Sci & Technol, Feuerwerkerstr 39, CH-3602 Thun, Switzerland
[3] ASCR, Inst Phys, Na Slovance 2, Prague 18221, Czech Republic
[4] HZG, Inst Werkstoffforsch, Notkestr 85, D-22547 Hamburg, Germany
[5] Alemnis GmbH, Feuerwerkerstr 39, CH-3602 Thun, Switzerland
[6] Safarik Univ, Dept Condensed Matter Phys, Pk Angelinum 9, Kosice, Slovakia
[7] Diamond Light Source Ltd, Harwell Sci & Innovat Campus, Didcot OX11 0DE, Oxon, England
关键词
DEFORMATION; INDENTATION; BEHAVIOR; FLOW;
D O I
10.1063/1.4939981
中图分类号
O59 [应用物理学];
学科分类号
摘要
A pioneer in-situ synchrotron X-ray nanodiffraction approach for characterization and visualization of strain fields induced by nanoindentation in amorphous materials is introduced. In-situ nanoindentation experiments were performed in transmission mode using a monochromatic and highly focused sub-micron X-ray beam on 40 mu m thick Zr-based bulk metallic glass under two loading conditions. Spatially resolved X-ray diffraction scans in the deformed volume of Zr-based bulk metallic glass covering an area of 40 x 40 mu m(2) beneath the pyramidal indenter revealed two-dimensional map of elastic strains. The largest value of compressive elastic strain calculated from diffraction data at 1 N load was -0.65%. The region of high elastic compressive strains (<-0.3%) is located beneath the indenter tip and has radius of 7 mu m. (C) 2016 AIP Publishing LLC.
引用
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页数:4
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