Ablation behavior and mechanism of SiC/Zr-Si-C multilayer coating for PIP-C/SiC composites under oxyacetylene torch flame

被引:18
作者
Xiang Yang [1 ]
Li Wei [1 ]
Wang Song [1 ]
Chen Zhao-hui [1 ]
Zhang Yan-zhi [1 ]
机构
[1] Natl Univ Def Technol, Sci & Technol Adv Ceram Fibers & Composites Lab, Changsha 410073, Hunan, Peoples R China
基金
中国国家自然科学基金;
关键词
Ceramic matrix composites (CMCs); Corrosion; High-temperature properties; Chemical vapor deposition (CVD); Molten salt; POLYCARBOSILANE; MICROSTRUCTURE; PYROLYSIS; CERAMICS;
D O I
10.1016/j.compositesb.2013.10.033
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
To improve the ablation resistance of PIP-C/SiC composites, SiC/Zr-Si-C multilayer coating was prepared by chemical vapor deposition (CVD) using methyltrichlorosilane (MTS) and hydrogen as the precursors and molten salt reaction using KCl-NaCl, sponge Zr and K2ZrF6, then the ablation capability of the coated composites was tested under oxyacetylene torch flame. The linear and mass ablation rates were much lower than those of uncoated samples. The linear and mass ablation rates of the three coating coated samples reached 0.0452 mm/s and 0.031 g/s, decreased by 27.3% and 27.1%, respectively. Moreover, the linear and mass ablation rates of the five coating coated samples reached 0.0255 mm/s and 0.0274 g/s, decreased by 59.0% and 35.5%. The gases released during ablation could take away a lot of heat, which was also helpful to the protection of the composites. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:127 / 132
页数:6
相关论文
共 14 条
[1]   Improved processing, and oxidation-resistance of ZrB2 ultra-high temperature ceramics containing SiC nanodispersoids [J].
Hwang, Sung S. ;
Vasiliev, Alexander L. ;
Padture, Nitin P. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2007, 464 (1-2) :216-224
[2]   Effects of pyrolysis processes on the microstructures and mechanical properties of Cf/SiC composites using polycarbosilane [J].
Jian, K ;
Chen, ZH ;
Ma, QS ;
Zheng, WW .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2005, 390 (1-2) :154-158
[3]   Effects of polycarbosilane infiltration processes on the microstructure and mechanical properties of 3D-Cf/SiC composites [J].
Jian, Ke ;
Chen, Zhao-Hui ;
Ma, Qing-Song ;
Hu, Hai-feng ;
Zheng, Wen-Wei .
CERAMICS INTERNATIONAL, 2007, 33 (06) :905-909
[4]   Stability of ultra-high-temperature ZrB2-SiC ceramics under simulated atmospheric re-entry conditions [J].
Monteverde, Frederic ;
Savino, Raffaele .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2007, 27 (16) :4797-4805
[5]   Finite element simulation of stress distribution and development of Cf/SiC ceramic-matrix composite coated with single layer SiC coating during thermal shock [J].
Wang, L. ;
Wang, Z. ;
Dong, S. M. ;
Zhang, W. ;
Wang, Y. .
COMPOSITES PART B-ENGINEERING, 2013, 51 :204-214
[6]   Fabrication of black-colored CuO-Al2O3-ZrO2 ceramics via heterogeneous nucleation method [J].
Wang, Wei ;
Liu, Wei ;
Yang, Xianfeng ;
Xie, Zhipeng .
CERAMICS INTERNATIONAL, 2012, 38 (04) :2851-2856
[7]   Preparation and properties of 2D C/ZrB2-SiC ultra high temperature ceramic composites [J].
Wang, Yiguang ;
Liu, Wen ;
Cheng, Laifei ;
Zhang, Litong .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 524 (1-2) :129-133
[8]  
Wei L, 2012, CERAM INT
[9]  
Yang X, 2013, COMPOSITES B, V45, P1391
[10]   Microstructure and ablation performances of dual-matrix carbon/carbon composites [J].
Yin, Jian ;
Xiong, Xiang ;
Zhang, Hongbo ;
Huang, Baiyun .
CARBON, 2006, 44 (09) :1690-1694