Small Magnets for Portable NMR Spectrometers

被引:152
作者
Danieli, Ernesto [1 ]
Perlo, Juan [1 ]
Bluemich, Bernhard [1 ]
Casanova, Federico [1 ]
机构
[1] Univ Aachen, Rhein Westfal TH Aachen, Inst Tech Chem & Makromol Chem, D-52074 Aachen, Germany
关键词
analytical methods; NMR spectroscopy; sensors; H-1; SPECTROSCOPY; SENSITIVITY; DESIGN; FIELDS; ARRAY;
D O I
10.1002/anie.201000221
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
(Figure Presented) Downsizing: A pocket-size permanent magnet has been constructed that is suitable for measuring 1H NMR spectra of samples in standard N MR tubes. The new shimming approach implemented to overcome the inherent inhomogeneity of permanent magnets opens the door to compact high-resolution NMR spectrometers for conventional samples. © 2010 Wiley-VCH Verlag GmbH & Co. KGaA.
引用
收藏
页码:4133 / 4135
页数:3
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共 15 条
  • [1] Reversible Interactions with para-Hydrogen Enhance NMR Sensitivity by Polarization Transfer
    Adams, Ralph W.
    Aguilar, Juan A.
    Atkinson, Kevin D.
    Cowley, Michael J.
    Elliott, Paul I. P.
    Duckett, Simon B.
    Green, Gary G. R.
    Khazal, Iman G.
    Lopez-Serrano, Joaqun
    Williamson, David C.
    [J]. SCIENCE, 2009, 323 (5922) : 1708 - 1711
  • [2] Mobile sensor for high resolution NMR spectroscopy and imaging
    Danieli, Ernesto
    Mauler, Joerg
    Perlo, Juan
    Bluemich, Bernhard
    Casanova, Federico
    [J]. JOURNAL OF MAGNETIC RESONANCE, 2009, 198 (01) : 80 - 87
  • [3] Portable, low-cost NMR with laser-lathe lithography produced microcoils
    Demas, Vasiliki
    Herberg, Julie L.
    Malba, Vince
    Bernhardt, Anthony
    Evans, Lee
    Harvey, Christopher
    Chinn, Sarah C.
    Maxwell, Robert S.
    Reimer, Jeffrey
    [J]. JOURNAL OF MAGNETIC RESONANCE, 2007, 189 (01) : 121 - 129
  • [4] DESIGN OF PERMANENT MULTIPOLE MAGNETS WITH ORIENTED RARE-EARTH COBALT MATERIAL
    HALBACH, K
    [J]. NUCLEAR INSTRUMENTS & METHODS, 1980, 169 (01): : 1 - 10
  • [5] A low-field, low-cost Halbach magnet array for open-access NMR
    Hills, BP
    Wright, KM
    Gillies, DG
    [J]. JOURNAL OF MAGNETIC RESONANCE, 2005, 175 (02) : 336 - 339
  • [6] SIGNAL-TO-NOISE RATIO OF NUCLEAR MAGNETIC-RESONANCE EXPERIMENT
    HOULT, DI
    RICHARDS, RE
    [J]. JOURNAL OF MAGNETIC RESONANCE, 1976, 24 (01) : 71 - 85
  • [7] Multipole shimming of permanent magnets using harmonic corrector rings
    Jachmann, R. C.
    Trease, D. R.
    Bouchard, L. -S.
    Sakellariou, D.
    Martin, R. W.
    Schlueter, R. D.
    Budinger, T. F.
    Pines, A.
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 2007, 78 (03)
  • [8] Chip-NMR biosensor for detection and molecular analysis of cells
    Lee, Hakho
    Sun, Eric
    Ham, Donhee
    Weissleder, Ralph
    [J]. NATURE MEDICINE, 2008, 14 (08) : 869 - 874
  • [9] Ultracompact NMR: 1H Spectroscopy in a Subkilogram Magnet
    McDowell, A.
    Fukushima, E.
    [J]. APPLIED MAGNETIC RESONANCE, 2008, 35 (01) : 185 - 195
  • [10] Miniature permanent magnet for table-top NMR
    Moresi, G
    Magin, R
    [J]. CONCEPTS IN MAGNETIC RESONANCE PART B-MAGNETIC RESONANCE ENGINEERING, 2003, 19B (01) : 35 - 43