α-Fe2O3 Hollow Spheres: Hydrothermal Synthesis and Phenol Adsorption Performance

被引：0

作者：

Yuan Xiao-Wei ^{[1
,2
]}

Yang Qian ^{[1
,2
]}

Liu Qi ^{[1
,2
,3
]}

Yu Li-Li ^{[1
,2
]}

Chen Qun ^{[1
,2
]}

Xu Zheng ^{[3
]}

机构：

[1] Jiangsu Polytech Univ, Sch Chem & Chem Engn, Changzhou 213164, Jiangsu, Peoples R China

[2] Jiangsu Polytech Univ, Jiangsu Prov Key Lab Fine Petrochem Technol, Changzhou 213164, Jiangsu, Peoples R China

[3] Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China

来源：

CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2010年 / 26卷 / 02期

关键词：

alpha-Fe2O3 hollow spheres; nanomaterials; adsorption; HEMATITE PARTICLES; CALCIUM-CARBONATE; FACILE SYNTHESIS; FABRICATION; MORPHOSYNTHESIS; NANOSTRUCTURES; NANOCRYSTALS; GROWTH; ION;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Using potassium ferricyanide, NH4H2PO4 as the reactants, alpha-Fe2O3 hollow spheres were synthesized by a hydrothermal method. The samples were characterized by TEM, MID, FESEM(field-emission scanning electron microscope), UV-Vis spectroscopy and low temperature nitrogen adsorption-desorption. The results show that the diameter of alpha-Fe2O3 hollow spheres is 200-560 run, and the BET surface area and the average diameter of pore is 80 m(2).g(-1) and 8.5 nm, respectively. The effect of the reaction time, the amount of reactant and the reaction temperature on the morphology and size of alpha-Fe2O3 hollow spheres was examined. The formation mechanism of the hollow spheres was proposed. The adsorption performance of alpha-Fe2O3 hollow spheres to phenol was investigated at room temperature, and the capacity for phenol adsorption was 97 mg.g(-1) when the balance of adsorption was reached.

引用

页码：285 / 292

页数：8

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