Tetrakis(tert-butyl 3-oxobutanoato)zirconium(IV)

被引：0

作者：

Urs, WJ

Dharmaprakash, MS

Shivashankar, SA

Row, TNG ^{[1
]}

机构：

[1] Indian Inst Sci, Solid State & Struct Chem Unit, Bangalore 560012, Karnataka, India

[2] Indian Inst Sci, Ctr Mat Res, Bangalore 560012, Karnataka, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷

关键词：

D O I：

10.1107/S1600536803002046

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The structure of the title compound, [Zr(C8H13O3)(4)], an MOCVD precursor, has been determined. The zirconium coordination geometry is dodecahedral and the chelate rings are significantly non-planar. The Zr atom lies on a (4) over bar axis, so the asymmetric unit contains only one ligand.

引用

页码：M83 / M84

页数：2

共 11 条

[1]

[Anonymous], 1993, CAMERON

[2]

Bruker, 2002, SMART SAINT

[3] REDETERMINATION OF THE STRUCTURE OF TETRAKIS(ACETYLACETONATO)ZIRCONIUM(IV) [J].

CLEGG, W .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1987, 43 :789-791

[4] ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI) [J].

Journal of Applied Crystallography, 1997, 30 (pt 5)

[5]

Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI [DOI 10.1107/S0021889899006020, 10.1107/S0021889899006020]

[6] STEREOCHEMISTRY OF DISCRETE 8-COORDINATION .1. BASIC ANALYSIS [J].

HOARD, JL ;

SILVERTON, JV .

INORGANIC CHEMISTRY, 1963, 2 (02) :235-&

[7]

Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]

[8]

Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR

[9]

Sheldrick G.M., 1996, SADABS VERSION 2008

[10] STEREOCHEMISTRY OF DISCRETE 8-COORDINATION .2. CRYSTAL AND MOLECULAR STRUCTURE OF ZIRCONIUM(IV) ACETYLACETONATE [J].

SILVERTON, JV ;

HOARD, JL .

INORGANIC CHEMISTRY, 1963, 2 (02) :243-&

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