Study of Physico-Chemical Properties and Growth Dimension Augmentation of Barium Succinate Single Crystals Grown by Slow Evaporation Technique

被引:3
作者
Christy, D. S. [1 ]
Shajan, Sahaya X. [2 ]
Mahadevan, C. K. [3 ]
机构
[1] St Johns Coll, Post Grad & Res Dept Phys, Tinmelveli 627002, Tamil Nadu, India
[2] PSN Coll Engn & Technol, Ctr Sci & Appl Res, Tirunelveli 627152, Tamil Nadu, India
[3] Bharathidasan Univ, Dept Phys, Tiruchirapuralli 620024, Tamil Nadu, India
关键词
x-ray diffraction; crystal growth from solution; barium compounds; mechanical hardness; dielectric materials; NLO crystal;
D O I
10.21315/jps2022.33.1.3
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Slow evaporation method was adopted to grow barium succinate (BS) single crystals for the first time and diamond shape crystals were successfully synthesised with dimension 14 mm(3) x 17 mm(3) x 4 mm(3). Single crystal x-ray diffraction studies show that the crystal system is monoclinic. Powder x-ray diffraction studies confirmed the crystallinity of the grown BS crystal. From energy dispersive x-ray spectroscopy (EDS) analysis the presence of barium metal was confirmed. The functional group of the BS crystal was confirmed from fourier transform infrared (FTIR) spectrum. The crystals were found to be hydrated and thermally stable up to 150 degrees C. BS crystal possesses good transmittance in the wavelength range 250 nm-1200 nm and it is non-linear optical (NLO) active material. The BS crystals have mechanical softness and normal dielectric behaviour.
引用
收藏
页码:29 / 49
页数:21
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