A facile green synthesis of silver nanoparticles using Piper betle biomass and its catalytic activity toward sensitive and selective nitrite detection

被引：67
|
作者：
Ramachandran, K. [1 ]
Kalpana, D. [2 ]
Sathishkumar, Y. [2 ]
Lee, Yang Soo [2 ]
Ravichandran, K. [3 ]
Kumar, G. Gnana [1 ]
机构：
[1] Madurai Kamaraj Univ, Sch Chem, Dept Phys Chem, Madurai 625021, Tamil Nadu, India
[2] Chonbuk Natl Univ, Inst Agr & Life Sci, Dept Forest Sci & Technol, Jeonju 561756, South Korea
[3] Anna Univ, Dept Rubber & Plast Technol, MIT Campus, Madras 600044, Tamil Nadu, India
来源：
JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY | 2016年 / 35卷
基金：
新加坡国家研究基金会;
关键词：
Biocompatible; Crystalline; Nitrite sensors; Reduction; Sensitivity; GLASSY-CARBON ELECTRODE; LEAF EXTRACT; GOLD NANOPARTICLES; ELECTROCHEMICAL DETERMINATION; FLOW-INJECTION; BIOSYNTHESIS; SENSOR; OXIDE; ION; ANTIOXIDANT;
D O I：
10.1016/j.jiec.2015.10.033
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A facile, one-pot and environmental benign method exploiting Piper betle biomass as a reducing and stabilizing agent was proposed for the preparation of silver (Ag) nanoparticles. The Ag nanoparticles prepared from dried Piper betle leaves extract exhibited unique spherical configuration and facecentered-cubic structure with preferred (1 1 1) orientation. The fabricated Ag/GCE sensor exhibited an exceptional electrocatalytic activity toward NO2- oxidation with a quick response time, high sensitivity and lower detection limit of 10 s, 1642.27 mu AmM-1 cm(-2) and 0.046 mu M, respectively. Furthermore, the constructed sensor exhibited long-term stability and excellent anti-interference properties, paving new dimensions for the utilization of bio-mediated nanocatalysts in electrochemical sensors. (C) 2015 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
引用
收藏
页码：29 / 35
页数：7
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