A comparison study of MFe2O4 (M: Ni, Cu, Zn)-reduced graphene oxide nanocomposite for electrochemical detection of bisphenol A

被引:55
作者
Bas, Salih Zeki [1 ]
Yuncu, Nese [1 ]
Atacan, Keziban [2 ]
Ozmen, Mustafa [1 ]
机构
[1] Selcuk Univ, Dept Chem, TR-42250 Konya, Turkey
[2] Sakarya Univ, Biomed Magnet & Semicond Mat Applicat & Res Ctr B, TR-54187 Sakarya, Turkey
关键词
Bisphenol A; Sensing application; Ferrite; Reduced graphene oxide; Screen-printed electrode; FERRITE NANOPARTICLES; ELECTROCATALYTIC ACTIVITY; SOLVOTHERMAL SYNTHESIS; HYDROTHERMAL SYNTHESIS; NIFE2O4; NANOPARTICLES; SENSOR; EFFICIENT; NANOSHEETS; WATER;
D O I
10.1016/j.electacta.2021.138519
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
In this work, the electrocatalytic activities and the sensing performances of a series of metal ferrites (MFe2O4, M: Ni, Cu, Zn) - reduced graphene oxide (rGO) nanocomposite (MFe2O4-rGO) prepared through a hydrothermal method were examined by using DPV, CV and EIS techniques. The electrochemical results exhibited that NiFe2O4-rGO nanocomposite modified screen-printed electrode (SPE) has a higher sensing performance towards the oxidation of bisphenol A (BPA) than those of the other ferrite (CuFe2O4, ZnFe2O4)-based SPEs. After optimizing crucial parameters such as accumulation time, accumulation potential and electrolyte pH, the DPV responses of NiFe2O4-rGO/SPE increased linearly with BPA concentration in the range of 0.05 mu M to 25 mu M (R-2 = 0.9976) with a low detection limit of 10 nM and a high sensitivity of 0.6132 mu A mu M-1. The specificity of the fabricated sensor towards BPA was assessed by analyzing the interference effect of some inorganic salt ions and phenol derivatives. In addition, the sensor prepared to detect BPA in the water bottle sample using only a few drops of the real sample diluted with 0.1 M phosphate buffer solution gave satisfactory responses. (C) 2021 Elsevier Ltd. All rights reserved.
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页数:8
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