Electrical characterization of BaTiO3 and Ba0.77Ca0.23TiO3 ceramics It synthesized by the proteic sol-gel method

被引:17
|
作者
Sampaio, D., V [1 ]
Silva, M. S. [1 ,2 ]
Souza, N. R. S. [1 ]
Santos, J. C. A. [1 ]
Rezende, M. V. S. [1 ]
Silva, R. S. [1 ]
机构
[1] Univ Fed Sergipe, Dept Fis, Grp Nanomat Funcionais, BR-49100000 Sao Cristovao, SE, Brazil
[2] Inst Fed Educ Ciencia & Tecnol Sertao Pernambucan, BR-56000000 Salgueiro, PE, Brazil
关键词
Barium titante; Sol-gel; Coconut water; Barium calcium titanate; Ceramic; Electrical properties; PHASE-TRANSITION; RELAXATION; CALCIUM;
D O I
10.1016/j.ceramint.2018.05.213
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this work, we introduce a simple, low-cost, and ecofriendly method for producing barium titanate (BaTiO3-BT) and barium calcium titanate (Ba0.77Ca0.23TiO3-BCT) powders. The synthesis was performed by using a proteic sol-gel route which use coconut water in the polymerization step of the metallic precursor. We investigated the effects of the processing parameters with the density, microstructure, and (di)electric properties as sample quality indicators. The sintered ceramics exhibit single crystalline phase, relative density of 95%, a homogeneous microstructure, and an average grain size of 4 m. The respective dielectric constants of 1200 (BT) and 700 (BCT), measured at room temperature, and the activation energy values for the conductive process are according to those reported in the literature for conventionally prepared ceramics.
引用
收藏
页码:15526 / 15530
页数:5
相关论文
共 50 条
  • [41] Electrical properties of sol-gel deposited BaTiO3 thin films on Si(100) substrates
    Cho, CR
    Kwun, SI
    Noh, TW
    Jang, MS
    JAPANESE JOURNAL OF APPLIED PHYSICS PART 1-REGULAR PAPERS BRIEF COMMUNICATIONS & REVIEW PAPERS, 1997, 36 (4A): : 2196 - 2199
  • [42] Effect of the processing temperature on the electrical properties of lead-free 0.965Bi0.5Na0.5TiO3-0.035BaTiO3 piezoelectric ceramics synthesized by sol-gel method
    Munir, Muhammad
    Habib, Muhammad
    Khan, Salman Ali
    Hussain, Ali
    Qazi, Ibrahim
    Choi, Yeon Bin
    Son, Jeong-Hun
    Malik, Rizwan Ahmad
    Bae, Dong-Sik
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2019, 90 (03) : 643 - 652
  • [43] Preparation and densification of BaTiO3 nanopowder by sol-gel autoigniting synthesis
    Hu, FR
    Li, L
    Zheng, DN
    Ge, CC
    JOURNAL OF UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING, 2002, 9 (03): : 188 - 192
  • [44] BaTiO3 thin films obtained by sol-gel spin coating
    Manso-Silván, A
    Fuentes-Cobas, L
    Martín-Palma, RJ
    Hernández-Vélez, M
    Martínez-Duart, JM
    SURFACE & COATINGS TECHNOLOGY, 2002, 151 : 118 - 121
  • [45] Sol-gel preparation of PZT thin films with BaTiO3 seeds
    Wu, AY
    Vilarinho, PM
    Salvado, IMM
    Baptista, JL
    THIRD INTERNATIONAL CONFERENCE ON THIN FILM PHYSICS AND APPLICATIONS, 1998, 3175 : 227 - 231
  • [46] Microstructure and electrical properties of (Ba,Sr)TiO3 thin films prepared by a sol-gel method
    Ren, TL
    Wang, XN
    Liu, JS
    Zhao, HJ
    Shao, TQ
    Liu, LT
    Li, ZJ
    INTEGRATED FERROELECTRICS, 2002, 45 : 13 - 21
  • [47] Dielectric behaviour of (Ba0.77Ca0.23)(Ti0.98Dy0.02)O3 ceramics
    Moquim, Abdul
    Panigrahi, Manas R.
    PROCESSING AND APPLICATION OF CERAMICS, 2015, 9 (02) : 91 - 98
  • [48] Optical properties of BaTiO3 and Mn:BaTiO3 thin films deposited on fused quartz and silicon substrates using a sol-gel method
    Li, YW
    Sun, JL
    Meng, XJ
    Zhang, WF
    Chu, JH
    FIFTH INTERNATIONAL CONFERENCE ON THIN FILM PHYSICS AND APPLICATIONS, 2004, 5774 : 168 - 171
  • [49] Er3+ and Yb3+ doped BaTiO3 powders and films prepared by sol-gel method
    Garcia-Murillo, Antonieta
    Garrido-Hernandez, Aristeo
    de Jesus Carrillo-Romo, Felipe
    Ivan Ceron-Montes, Genaro
    JOURNAL OF THE AUSTRALIAN CERAMIC SOCIETY, 2018, 54 (02) : 345 - 355
  • [50] Er3+ and Yb3+ doped BaTiO3 powders and films prepared by sol-gel method
    Antonieta García-Murillo
    Aristeo Garrido-Hernández
    Felipe de Jésus Carrillo-Romo
    Genaro Iván Cerón-Montes
    Journal of the Australian Ceramic Society, 2018, 54 : 345 - 355