Formation of niobium oxide nanowires by thermal oxidation

被引：26

作者：

Lim, Jae Hoon ^{[2
]}

Choi, Jinsub ^{[1
]}

机构：

[1] Inha Univ, Dept Chem Engn, Nanostruct Mat Res Lab, Inchon 402751, South Korea

[2] BioBud Inc, Seoul 153777, South Korea

来源：

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY | 2009年 / 15卷 / 06期

关键词：

Annealing; Nanowires; Metal oxides; Niobium oxide; Valve metal; CHEMICAL-VAPOR-DEPOSITION; NANOSTRUCTURES; NB2O5; FILMS; ZNO; CATALYSIS; EMISSION; TITANIUM; CU2O; AIR;

D O I：

10.1016/j.jiec.2009.09.013

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In this report, we describe simple thermal oxidation of niobium for the fabrication of niobium oxides, emphasizing that niobium oxide nanowires can be prepared upon the concentration of oxygen in the environment. For example, dense Nb2O5 nanowires on thin oxide film are produced if the annealing is performed in a restricted concentration of oxygen (herein, 3 Torr vacuum). If most of the oxygen is removed in the environment, the nanowires are sparely formed. The nanowires consist of a superlattice monoclinic Nb2O5 with a growth direction of [0 0 1]. (C) 2009 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.

引用

页码：860 / 864

页数：5

共 27 条

[1] Synthesis of a stable hexagonally packed mesoporous niobium oxide molecular sieve through a novel ligand-assisted templating mechanism [J].

Antonelli, DM ;

Ying, JY .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1996, 35 (04) :426-430

[2] Plasmon-assisted chemical vapor deposition [J].

Boyd, David A. ;

Greengard, Leslie ;

Brongersma, Mark ;

El-Naggar, Mohamed Y. ;

Goodwin, David G. .

NANO LETTERS, 2006, 6 (11) :2592-2597

[3] Porous niobium oxide films prepared by anodization in HF/H3PO4 [J].

Choi, Jinsub ;

Lim, Jae Hoon ;

Lee, Sang Cheon ;

Chang, Jeong Ho ;

Kim, Kyung Ja ;

Cho, Min Ae .

ELECTROCHIMICA ACTA, 2006, 51 (25) :5502-5507

[4] Multifunctional nanowire bioscaffolds on titanium [J].

Dong, Wenjun ;

Zhang, Tierui ;

Epstein, Joshua ;

Cooney, Lisa ;

Wang, Hong ;

Li, Yanbin ;

Jiang, Ying-Bing ;

Cogbill, Andrew ;

Varadan, Vijay ;

Tian, Z. Ryan .

CHEMISTRY OF MATERIALS, 2007, 19 (18) :4454-4459

[5] CuO nanowires can be synthesized by heating copper substrates in air [J].

Jiang, XC ;

Herricks, T ;

Xia, YN .

NANO LETTERS, 2002, 2 (12) :1333-1338

[6] Niobium pentoxide as a lean-range oxygen sensor [J].

Kohli, A ;

Wang, CC ;

Akbar, SA .

SENSORS AND ACTUATORS B-CHEMICAL, 1999, 56 (1-2) :121-128

[7] Chemical sensing and catalysis by one-dimensional metal-oxide nanostructures [J].

Kolmakov, A ;

Moskovits, M .

ANNUAL REVIEW OF MATERIALS RESEARCH, 2004, 34 :151-180

[8] Novel solvothermal synthesis of niobium(v) oxide powders and their photocatalytic activity in aqueous suspensions [J].

Kominami, H ;

Oki, K ;

Kohno, M ;

Onoue, S ;

Kera, Y ;

Ohtani, B .

JOURNAL OF MATERIALS CHEMISTRY, 2001, 11 (02) :604-609

[9]

Lee J, 2004, J IND ENG CHEM, V10, P1058

[10] Field emission and photofluorescent characteristics of zinc oxide nanowires synthesized by a metal catalyzed vapor-liquid-solid process [J].

Li, SY ;

Lin, P ;

Lee, CY ;

Tseng, TY .

JOURNAL OF APPLIED PHYSICS, 2004, 95 (07) :3711-3716

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