Synthesis and crystal structure of ethyl 4-(4-nitrobenzamido)-3-(N-methyl-4-nitrobenzamido)-benzoate monohydrate

被引：0

作者：

Li, Xue-Mei ^{[1
]}

Zhang, Fan ^{[1
]}

Du, Li-Ping ^{[1
]}

Zhang, Shu-Sheng ^{[1
]}

机构：

[1] Qingdao Univ Sci & Technol, Coll Chem & Mol Engn, Qingdao 266042, Peoples R China

来源：

ASIAN JOURNAL OF CHEMISTRY | 2007年 / 19卷 / 05期

关键词：

4-(4-nitrobenzamido)-3-(N-methyl-4-nitrobenzamido) benzoate monohydrate; crystal structure; synthesis;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In this article, ethyl 4-(4-Nitrobenzamido)-3-(N-methyl-4-nitrobenzamido)benzoate monohydrate was synthesized through the reaction of 4-nitrobenzoyl chloride and 3,4-diamino benzoate using Et3N as acid acceptor. The structure of the present compound was characterized using elemental analysis, IR, H-1 NMR spectra and X-ray crystallography. The compound crystallizes in the triclinic system, space group P-1, with cell dimensions of a =7.394(6), b = 11.418(8), c = 14.293 (11)angstrom, alpha = 84.1-32(13), beta = 81.034(13), gamma = 89.451(13)degrees, V = 1185.7(.16) angstrom(3) and Z = 2.

引用

页码：3923 / 3928

页数：6

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