Fabrication of Ti3AlC2 powder with high-purity by pressureless sintering

被引：15

作者：

Peng, CQ ^{[1
]}

Wang, CA ^{[1
]}

Qi, L ^{[1
]}

Huang, Y ^{[1
]}

机构：

[1] Tsing Hua Univ, State Key Lab New Ceram & Fine Proc, Dept Mat Sci & Engn, Beijing 100084, Peoples R China

来源：

PRICM 5: THE FIFTH PACIFIC RIM INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS AND PROCESSING, PTS 1-5 | 2005年 / 475-479卷

关键词：

Ti3AlC2; powder; high-purity; B2O3; pressureless synthesis;

D O I：

10.4028/www.scientific.net/MSF.475-479.1247

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

In this work, a new method to fabricate high-purity Ti3AlC2 powder by pressureless sintering (PLS) was reported through adding a little amount of B2O3 as a low-temperature aid. The elemental Ti, Al, and active carbon powders were used as raw materials with the molar ratio of 3 : 1.2 : 2. The effect of sintering temperature on the purity of Ti3AlC2 was investigated at the range of 800 degrees C to 1400 degrees C. The results showed that high-purity Ti3AlC2 powders, in which almost no TiC phase could be found, were stably fabricated by pressureless synthesis at 1400 degrees C for 5 mins in flow Ar atmosphere. The roles of B2O3 addition were discussed in the paper.

引用

页码：1247 / 1250

页数：4

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