Influence of the sintering temperature on ferroelectric properties of potassium-sodium niobate piezoelectric

被引:6
作者
Cortes, J. A. [1 ]
Camargo, J. [2 ]
Rachia, M. F. [1 ]
Rubio-Marcos, F. [3 ,4 ]
Ramajo, L. [2 ]
Castro, M. [2 ]
Ramirez, M. A. [1 ]
机构
[1] Sao Paulo State Univ UNESP, Fac Engn Guaratingueta, Av Dr Ariberto Pereira Cunha 333, BR-12516410 Guaratingueta, SP, Brazil
[2] INTEMA, Res Inst Mat Sci & Technol, Av Colon 10850,B7608FDQ, Mar Del Plata, Argentina
[3] CSIC, Electroceram Dept, Inst Ceram & Vidrio, Kelsen 5, Madrid 28049, Spain
[4] Univ Antonio Nebrija, Escuela Politecn Super, Pirineos 55, Madrid 28040, Spain
关键词
KNL-NTS; lead-free; ferroelectric properties; ELECTRICAL-PROPERTIES; PHASE-STRUCTURE; SOL-GEL; PIEZOCERAMICS; EVOLUTION; POWDERS; TA;
D O I
10.1142/S2010135X21400026
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The effect of sintering condition on structure, microstructure, and ferroelectric properties of (K0.44Na0.52Li0.04) (Nb0.86Ta0.10Sb0.04)-O-3 (KNL-NTS) has been investigated. Ceramic powders have been synthesized by the solid-state reaction method and sintered at different temperatures (1115 degrees C, 1125 degrees C, and 1140 degrees C). Then, samples were characterized by thermogravimetric analysis, X-ray diffraction, scanning electron microscopy, and impedance spectroscopy. Through XRD results, the perovskite structure and small peaks corresponding to a secondary phase were detected. Ceramics processed at the highest temperatures showed higher densities and good piezoelectric properties (d(33), K-p, and K-t), particularly specimens sintered at 1125 degrees C presented the highest piezoelectric performance.
引用
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页数:8
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