Hard x-ray nanobeam characterization by coherent diffraction microscopy

被引:149
作者
Schropp, A. [1 ]
Boye, P. [1 ]
Feldkamp, J. M. [1 ]
Hoppe, R. [1 ]
Patommel, J. [1 ]
Samberg, D. [1 ]
Stephan, S. [1 ]
Giewekemeyer, K. [2 ]
Wilke, R. N. [2 ]
Salditt, T. [2 ]
Gulden, J. [3 ]
Mancuso, A. P. [3 ]
Vartanyants, I. A. [3 ]
Weckert, E. [3 ]
Schoeder, S. [4 ]
Burghammer, M. [4 ]
Schroer, C. G. [1 ]
机构
[1] Tech Univ Dresden, Inst Struct Phys, D-01062 Dresden, Germany
[2] Univ Gottingen, Inst Xray Phys, D-37077 Gottingen, Germany
[3] Deutsch Elektronen Synchrotron DESY, D-22607 Hamburg, Germany
[4] European Synchrotron Radiat Facil, F-38043 Grenoble, France
关键词
statistics; X-ray diffraction; X-ray microscopy; PHASE RETRIEVAL; RESOLUTION;
D O I
10.1063/1.3332591
中图分类号
O59 [应用物理学];
学科分类号
摘要
We have carried out a ptychographic scanning coherent diffraction imaging experiment on a test object in order to characterize the hard x-ray nanobeam in a scanning x-ray microscope. In addition to a high resolution image of the test object, a detailed quantitative picture of the complex wave field in the nanofocus is obtained with high spatial resolution and dynamic range. Both are the result of high statistics due to the large number of diffraction patterns. The method yields a complete description of the focus, is robust against inaccuracies in sample positioning, and requires no particular shape or prior knowledge of the test object.
引用
收藏
页数:3
相关论文
共 20 条
[1]   Probing the structure of heterogeneous diluted materials by diffraction tomography [J].
Bleuet, Pierre ;
Welcomme, Eleonore ;
Dooryhee, Eric ;
Susini, Jean ;
Hodeau, Jean-Louis ;
Walter, Philippe .
NATURE MATERIALS, 2008, 7 (06) :468-472
[2]   Nano-imaging of trace metals by synchrotron X-ray fluorescence into dopaminergic single cells and neurite-like processes [J].
Carmona, Asuncion ;
Cloetens, Peter ;
Deves, Guillaume ;
Bohic, Sylvain ;
Ortega, Richard .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 2008, 23 (08) :1083-1088
[3]   Soft X-ray microscopy at a spatial resolution better than 15nm [J].
Chao, WL ;
Harteneck, BD ;
Liddle, JA ;
Anderson, EH ;
Attwood, DT .
NATURE, 2005, 435 (7046) :1210-1213
[4]  
CHU S, 2008, APPL PHYS LETT, V92
[5]   Phase retrieval with transverse translation diversity: a nonlinear optimization approach [J].
Guizar-Sicairos, Manuel ;
Fienup, James R. .
OPTICS EXPRESS, 2008, 16 (10) :7264-7278
[6]   Measurement of coherent x-ray focused beams by phase retrieval with transverse translation diversity [J].
Guizar-Sicairos, Manuel ;
Fienup, James R. .
OPTICS EXPRESS, 2009, 17 (04) :2670-2685
[7]   Nanometer linear focusing of hard x rays by a multilayer Laue lens [J].
Kang, HC ;
Maser, J ;
Stephenson, GB ;
Liu, C ;
Conley, R ;
Macrander, AT ;
Vogt, S .
PHYSICAL REVIEW LETTERS, 2006, 96 (12)
[8]   Focusing of hard x-rays to 16 nanometers with a multilayer Laue lens [J].
Kang, Hyon Chol ;
Yan, Hanfei ;
Winarski, Robert P. ;
Holt, Martin V. ;
Maser, Joerg ;
Liu, Chian ;
Conley, Ray ;
Vogt, Stefan ;
Macrander, Albert T. ;
Stephenson, G. Brian .
APPLIED PHYSICS LETTERS, 2008, 92 (22)
[9]   Visualizing a Catalyst at Work during the Ignition of the Catalytic Partial Oxidation of Methane [J].
Kimmerle, Bertram ;
Grunwaldt, Jan-Dierk ;
Baiker, Alfons ;
Glatzel, Pieter ;
Boye, Pit ;
Stephan, Sandra ;
Schroer, Christian G. .
JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 113 (08) :3037-3040
[10]   An improved ptychographical phase retrieval algorithm for diffractive imaging [J].
Maiden, Andrew M. ;
Rodenburg, John M. .
ULTRAMICROSCOPY, 2009, 109 (10) :1256-1262