Influence of stabilizing agents on structural and optical properties of cobalt oxide nanoparticles synthesized by an ultrasound-assisted method

被引:5
|
作者
Mammadyarova, S. J. [1 ]
Muradov, M. B. [1 ]
Maharramov, A. M. [2 ]
Eyvazova, G. M. [1 ]
Aghamaliyev, Z. A. [1 ]
Balayeva, O. O. [2 ]
Hasanova, I. [2 ]
机构
[1] Baku State Univ, Dept Phys, Z Khalilov Str 23, AZ-1148 Baku, Azerbaijan
[2] Baku State Univ, Dept Chem, Baku, Azerbaijan
关键词
Band gap; cobalt oxide; stabilizing agent; CO3O4; NANOCRYSTALS; PHASE; NANOFIBERS; COO;
D O I
10.1080/00387010.2019.1686396
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
Cobalt oxide nanoparticles were synthesized using a facile and convenient sonochemical method, followed by a calcination process. For the synthesis, cobalt nitrate, and sodium borohydride were used as precursors. Polyvinyl alcohol, 3-mercaptopropionic acid, and styrene were used as a stabilizing agent. To identify the structure, optical properties and morphology, the synthesized nanoparticles were characterized using X-ray diffraction, Ultraviolet-Visible Spectroscopy, Fourier-transform infrared spectroscopy, transmission electron microscopy, and scanning electron microscopy. To explain the formation mechanism of cobalt oxide nanoparticles, some investigations were carried out before thermal annealing. In addition, the particle size was tuned by variation of the concentration of 3-mercaptopropionic acid.
引用
收藏
页码:677 / 686
页数:10
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