Strain analysis by inversion of coherent Bragg X-ray diffraction intensity: the illumination problem

被引:5
作者
Chamard, V. [1 ]
Dolle, M. [2 ]
Baldinozzi, G. [3 ]
Livet, F. [4 ]
de Boissieu, M. [4 ]
Labat, S. [1 ]
Picca, F. [1 ,5 ]
Mocuta, C. [5 ]
Donnadieu, P. [4 ]
Metzger, T. H. [6 ]
机构
[1] Univ Aix Marseille, CNRS, IM2NP, F-13397 Marseille 20, France
[2] CNRS, CEMES, F-31055 Toulouse, France
[3] Ecole Cent Paris, SPMS, F-92295 Chatenay Malabry, France
[4] SIMaP, F-38402 St Martin Dheres, France
[5] LOrme Merisiers St Aubin, Synchrotron Soleil, F-91192 Gif Sur Yvette, France
[6] European Synchrotron Radiat Facil, F-38043 Grenoble, France
关键词
inversion problem; coherent X-ray diffraction; strain analysis; nano-crystals; nano-focusing; PHASE; NANOCRYSTALS; MICROSCOPY; ALGORITHM; CRYSTAL;
D O I
10.1080/09500341003746645
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
Bragg coherent X-ray diffraction imaging is demonstrated with a micro-focused illumination. The 2D projected density of the 3D nano-crystal is successfully retrieved from the inversion of its diffraction intensity pattern. The analysis of the phase field at the sample position, which holds in principle the strain information, emphasizes the high sensitivity of the technique with regard to the wavefront structure. The ptychography approach is a proposed solution to discriminate the wavefront function from the sample electron density distribution. It is based on a redundancy of the collected information obtained by measuring a series of diffraction patterns for different but overlapping beam positions onto the sample. Applicability to the Bragg geometry still needs to be demonstrated.
引用
收藏
页码:816 / 825
页数:10
相关论文
共 40 条
[1]  
[Anonymous], 1963, XRAY STUDIES MAT
[2]   Three-dimensional coherent x-ray diffraction imaging of a ceramic nanofoam: Determination of structural deformation mechanisms [J].
Barty, A. ;
Marchesini, S. ;
Chapman, H. N. ;
Cui, C. ;
Howells, M. R. ;
Shapiro, D. A. ;
Minor, A. M. ;
Spence, J. C. H. ;
Weierstall, U. ;
Ilavsky, J. ;
Noy, A. ;
Hau-Riege, S. P. ;
Artyukhin, A. B. ;
Baumann, T. ;
Willey, T. ;
Stolken, J. ;
van Buuren, T. ;
Kinney, J. H. .
PHYSICAL REVIEW LETTERS, 2008, 101 (05)
[3]   Stuctural investigation of InAs nanowires with coherent X-rays [J].
Chamard, V. ;
Diaz, A. ;
Stangl, J. ;
Labat, S. .
JOURNAL OF STRAIN ANALYSIS FOR ENGINEERING DESIGN, 2009, 44 (07) :533-542
[4]   Coherent diffraction imaging of a single epitaxial InAs nanowire using a focused x-ray beam [J].
Diaz, A. ;
Mocuta, C. ;
Stangl, J. ;
Mandl, B. ;
David, C. ;
Vila-Comamala, J. ;
Chamard, V. ;
Metzger, T. H. ;
Bauer, G. .
PHYSICAL REVIEW B, 2009, 79 (12)
[5]   Coherence and wavefront characterization of Si-111 monochromators using double-grating interferometry [J].
Diaz, Ana ;
Mocuta, Cristian ;
Stangl, Julian ;
Keplinger, Mario ;
Weitkamp, Timm ;
Pfeiffer, Franz ;
David, Christian ;
Metzger, Till H. ;
Bauer, Guenther .
JOURNAL OF SYNCHROTRON RADIATION, 2010, 17 :299-307
[6]   Imaging the displacement field within epitaxial nanostructures by coherent diffraction: a feasibility study [J].
Diaz, Ana ;
Chamard, Virginie ;
Mocuta, Cristian ;
Magalhaes-Paniago, Rogerio ;
Stangl, Julian ;
Carbone, Dina ;
Metzger, Till H. ;
Bauer, Guenther .
NEW JOURNAL OF PHYSICS, 2010, 12
[7]   Synthesis of nanosized zirconium carbide by a sol-gel route [J].
Dolle, Mickael ;
Gosset, Dominique ;
Bogicevic, Christine ;
Karolak, Fabienne ;
Simeone, D. ;
Baldinozzi, G. .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2007, 27 (04) :2061-2067
[8]   Movable aperture lensless transmission microscopy: A novel phase retrieval algorithm [J].
Faulkner, HML ;
Rodenburg, JM .
PHYSICAL REVIEW LETTERS, 2004, 93 (02) :023903-1
[9]   Coherent-diffraction imaging of single nanowires of diameter 95 nanometers [J].
Favre-Nicolin, Vincent ;
Eymery, Joel ;
Koester, Robert ;
Gentile, Pascal .
PHYSICAL REVIEW B, 2009, 79 (19)
[10]   PHASE RETRIEVAL ALGORITHMS - A COMPARISON [J].
FIENUP, JR .
APPLIED OPTICS, 1982, 21 (15) :2758-2769