2D full-field measurement of oxygen concentration based on the phase fluorometry technique that uses the four-frame integrating-bucket method

被引:8
作者
Chu, Chen-Shane [1 ]
Lo, Yu-Lung [1 ]
机构
[1] Natl Cheng Kung Univ, Dept Mech Engn, Tainan 70101, Taiwan
关键词
Full-field; Oxygen sensor; Phase fluorometry; Pt(II) complex; Sol-gel; HETERODYNE POLARISCOPE; FLUORESCENCE; DOMAIN; RETARDATION; MICROSCOPY; SENSORS; AXIS; PH;
D O I
10.1016/j.snb.2010.03.032
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A modulation system for the phase-resolved two-dimensional fluorescence phase imaging of a planar optical oxygen sensor is presented. The proposed system is based on the phase fluorometry technique and uses the four-frame integrating-bucket method. Integrating buckets with multiple frames are achieved using a complex programmable logic device to provide an external trigger to the charge coupled device (CCD). The oxygen-sensitive film is based on microporous film prepared using a sol-gel process with a NW complex, platinum tetrakis pentafluorophenyl porphine (PtTFPP); the film can be efficiently excited by a laser diode with a central wavelength of 405 nm. The experiment results show that the maximum phase difference between 0% and 100% gaseous oxygen is 22 degrees. The 2D full-filed O-2 distribution imaging was found to be the most sensitive between 0% and 20% O-2. The combination of optical sensor technology and phase-resolved imaging allows the determination of the distribution of chemical or physical parameters in heterogeneous systems, making the proposed system a powerful testing tool for screening and mapping applications. (c) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:310 / 315
页数:6
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