Synthesis, Characterization and Thermal Behaviors of 4-Amino-5-nitro-1,2,3-triazole (ANTZ) and Its Derivatives

被引：11

作者：

Wang Bozhou ^{[1
]}

Li Jizhen ^{[1
]}

Huo Huan ^{[1
]}

Fan Xuezhong ^{[1
]}

Fu Xiaolong ^{[1
]}

Zhou Cheng ^{[1
]}

机构：

[1] Xian Modern Chem Res Inst, Xian 710065, Shaanxi, Peoples R China

来源：

CHINESE JOURNAL OF CHEMISTRY | 2010年 / 28卷 / 05期

关键词：

organic chemistry; synthesis; 4-amino-5-nitro-1,2,3-triazole; thermolysis;

D O I：

10.1002/cjoc.201090146

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

4-Amino-5-nitro-1,2,3-triazole (ANTZ) and its derivatives, such as 2-(4-amino-5-nitro-1,2,3-trazole-1-yl)-1,3,5-trinitrobenzene (T-ANTZ) and 4-amino-5-nitro-1,2,3-triazole (M-ANTZ), were synthesized and characterized, whose structures were confirmed by IR, NMR and elemental analysis. The thermal behaviors of ANTZ, T-ANTZ and M-ANTZ were studied by the methods of DSC and TG-DTG, and the results showed that there is an obvious melting, process of ANTZ with melting point of 278.38 degrees C, while there is no melting process in the thermal behavior of T-ANTZ and M-ANTZ (the derivatives of ATNZ).

引用

页码：781 / 784

页数：4

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