A comparative study of the pressureless sinterability of 3 mol% Y2O3-stabilized ZrO2 powders prepared by the sol-gel method under different synthesis conditions without modifiers

被引：6

作者：

Mamana, Nadia ^{[1
]}

Ortiz, Angel L. ^{[2
]}

Sanchez-Bajo, Florentino ^{[3
]}

Caruso, Ricardo ^{[1
]}

机构：

[1] UNR, CONICET, Inst Fis Rosario, Lab Mat Ceram, RA-2000 Rosario, Santa Fe, Argentina

[2] Univ Extremadura, Dept Ingn Mecan Energet & Mat, Badajoz 06006, Spain

[3] Univ Extremadura, Dept Fis Aplicada, Badajoz 06006, Spain

来源：

CERAMICS INTERNATIONAL | 2014年 / 40卷 / 10期

关键词：

ZrO2; Sol-gel; Powder; Microstructure; Densification; YTTRIA-STABILIZED ZIRCONIA; PHASE-TRANSFORMATION; TETRAGONALITY; PARAMETERS; PARTICLES;

D O I：

10.1016/j.ceramint.2014.08.015

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

A wide set of 3 mol% Y2O3-stabilized ZrO2 (3YSZ) powders have been synthesized by the sol-gel method without modifiers from solutions of zirconium n-propoxide and yttrium acetate prepared with different water/Zr molar ratio and zirconium concentration, and the effect of these two synthesis variables on the pressureless sinterability of the 3YSZ powders has been investigated. It was found that the sinterability increases with increasing zirconium concentration and water/Zr molar ratio, which is attributed to the smaller cluster size developed during the sol-gel synthesis. Implications for the preparation of more sinterable 3YSZ powders are discussed. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

引用

页码：16829 / 16834

页数：6

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