Deep Learning Based Instance Segmentation of Titanium Dioxide Particles in the Form of Agglomerates in Scanning Electron Microscopy

被引:32
作者
Monchot, Paul [1 ]
Coquelin, Loic [1 ]
Guerroudj, Khaled [1 ]
Feltin, Nicolas [2 ]
Delvallee, Alexandra [2 ]
Crouzier, Loic [2 ]
Fischer, Nicolas [1 ]
机构
[1] Data Sci & Uncertainty Dept, Natl Lab Metrol & Testing, 29 Ave Roger Hennequin, F-78197 Trappes, France
[2] Dept Mat Sci, Natl Lab Metrol & Testing, 29 Ave Roger Hennequin, F-78197 Trappes, France
关键词
scanning electron microscopy; mask R-CNN; deep learning; particle size distribution; instance segmentation; TiO2; agglomerate; IMAGE; SEARCH; AFM; SEM;
D O I
10.3390/nano11040968
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The size characterization of particles present in the form of agglomerates in images measured by scanning electron microscopy (SEM) requires a powerful image segmentation tool in order to properly define the boundaries of each particle. In this work, we propose to use an algorithm from the deep statistical learning community, the Mask-RCNN, coupled with transfer learning to overcome the problem of generalization of the commonly used image processing methods such as watershed or active contour. Indeed, the adjustment of the parameters of these algorithms is almost systematically necessary and slows down the automation of the processing chain. The Mask-RCNN is adapted here to the case study and we present results obtained on titanium dioxide samples (non-spherical particles) with a level of performance evaluated by different metrics such as the DICE coefficient, which reaches an average value of 0.95 on the test images.
引用
收藏
页数:17
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