Small-angle X-ray scattering at the ESRF high-brilliance beamline

被引:43
作者
Bosecke, P [1 ]
Diat, O [1 ]
机构
[1] European Synchrotron Radiat Facil, F-38043 Grenoble, France
关键词
D O I
10.1107/S0021889897001647
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The high-brilliance beamline (BL4/ID2) at the European Synchrotron Radiation Facility (ESRF) in Grenoble has been constructed with the emphasis on time-resolved small-angle X-ray scattering and macromolecular crystallography. It has been open to users for two years. The beamline has opened up new areas in small-angle scattering research, facilitating (a) small-angle crystallography on structures with unit cells of several hundredths of nanometres, (b) overlap with the light scattering range for the study of optical systems, (c) high photon flux for time-resolved experiments and (d) a high spatial coherence allowing submicrometre imaging with X-rays. The set-up and the detector system of the small-angle scattering station are presented. A method for obtaining absolute scattering intensities is described. The parasitic background at the station is discussed in terms of absolute scattering intensities.
引用
收藏
页码:867 / 871
页数:5
相关论文
共 20 条
[1]   A FAST READOUT SYSTEM FOR 2D GAS-FILLED DETECTORS BASED ON THE DELAY-LINE METHOD [J].
BERRY, A ;
GABRIEL, A ;
KOCSIS, M ;
RIEKEL, C .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1994, 348 (2-3) :334-337
[2]  
BOSECKE P, 1992, REV SCI INSTRUM, V63, P438, DOI 10.1063/1.1142724
[3]   HIGH-BRILLIANCE BEAMLINE AT THE EUROPEAN SYNCHROTRON-RADIATION FACILITY [J].
BOSECKE, P ;
DIAT, O ;
RASMUSSEN, B .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02) :1636-1638
[4]  
BOSECKE P, 1997, UNPUB
[5]   DATA ACQUISITION-SYSTEMS FOR LINEAR AND AREA X-RAY-DETECTORS USING DELAY-LINE READOUT [J].
BOULIN, CJ ;
KEMPF, R ;
GABRIEL, A ;
KOCH, MHJ .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1988, 269 (01) :312-320
[6]   Pressure-induced stabilization of the smectic A* phase in a chiral polyacrylate [J].
Caciuffo, R ;
Francescangeli, O ;
Paci, B ;
Bosecke, P ;
Ferrero, C ;
Lorenzen, M .
EUROPHYSICS LETTERS, 1996, 34 (07) :501-506
[7]  
Dobbie I, 1996, J MUSCLE RES CELL M, V17, P163
[8]   LIQUID-CRYSTALLINE SIDE-GROUP BLOCK-COPOLYMERS WITH N-BUTYL METHACRYLATE AS AN AMORPHOUS A-BLOCK - SYNTHESIS AND CHARACTERIZATION [J].
FISCHER, H ;
POSER, S ;
ARNOLD, M .
MACROMOLECULES, 1995, 28 (20) :6957-6962
[9]   Comparison of parasitic scattering from window materials used for small-angle X-ray scattering: A better beryllium window [J].
Henderson, SJ .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1995, 28 :820-826
[10]  
HENDRIX J, 1985, ADV POLYM SCI, V67